反应条件
1.1: magnesium / diethyl ether
1.2: Cooling with ice; Reflux
2.1: pyridine / dichloromethane / 20 °C / Inert atmosphere
3.1: 2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride / hexane / 25 °C / Cooling with liquid nitrogen; Sealed tube; UV-irradiation
View Scheme
参考文献
Beckwith, Athelstan L. J.; Schiesser, Carl H.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 6 p. 1736 - 1743
