(1-氧代-1,3-二氢异苯并呋喃-5-基)羰酰氯合成路线 (共 9 条)
反应条件
thionyl chloride; N,N-dimethyl-formamide T=60°C; 3 - 5 h; Heating / reflux; Product distribution / selectivity;
参考文献
Adorkem Technology SpA
Patent: EP1777221 A1, 2007 ;
Location in patent: Page/Page column 4-5 ;
反应条件
thionyl chloride in n-heptane; toluene
参考文献
H. Lundbeck A/S
Patent: US2002/19546 A1, 2002 ;
反应条件
1: copper (II)-sulfate; potassium cyanide / ueber eine wss. Diazoniumsalz-Loesung 2: aqueous sulfuric acid 3: aq. NaOH solution / anschliessend Ansaeuern 4: thionyl chloride View Scheme
参考文献
Levy; Stephen
Journal of the Chemical Society, 1931 , p. 867,869
反应条件
1: aqueous sulfuric acid 2: aq. NaOH solution / anschliessend Ansaeuern 3: thionyl chloride View Scheme
参考文献
Levy; Stephen
Journal of the Chemical Society, 1931 , p. 867,869
反应条件
1: aq. NaOH solution / anschliessend Ansaeuern 2: thionyl chloride View Scheme
参考文献
Levy; Stephen
Journal of the Chemical Society, 1931 , p. 867,869
反应条件
triethylamine in tetrahydrofuran
参考文献
H. Lundbeck A/S
Patent: US2002/40153 A1, 2002 ;
反应条件
amidosulfamic acid in sulfolane; water
参考文献
H. Lundbeck A/S
Patent: US2002/28956 A1, 2002 ;
反应条件
ammonium hydroxide in N,N-dimethyl acetamide
参考文献
INFOSINT SA
Patent: EP1281708 A1, 2003 ;
参考文献
Levy; Stephen
Journal of the Chemical Society, 1931 , p. 867,869