2,3-二氢-5,6-二甲基-1,4-二噻英合成路线 （共 9 条）
反应条件
toluene-4-sulfonic acid in water; toluene
参考文献
Uniroyal Ltd.
Patent: US4319033 A1, 1982 ;
反应条件
bromine in tetrachloromethane 0.333333 h; Ambient temperature;
参考文献
Caputo, Romualdo; Ferreri, Carla; Palumbo, Giovanni; Capozzi, Giuseppe
Tetrahedron, 1986 , vol. 42, # 8 p. 2369 - 2376
反应条件
hydrogenchloride; toluene-4-sulfonic acid in water; benzene
参考文献
Uniroyal Inc.; Uniroyal, Ltd.
Patent: US3997323 A1, 1976 ;
反应条件
toluene-4-sulfonic acid in benzene 23 h; Heating;
参考文献
Russell,G.A.; Law,W.C.; Zaleta,M.
Journal of the American Chemical Society, 1985 , vol. 107, p. 4175
反应条件
tris-(2-chloro-ethyl)-amine; thiamine diphosphate; diethylazodicarboxylate in benzene T=20°C; Azide formation; 72 h;
参考文献
Afonso, Carlos A. M.; Barros, M. Teresa; Maycock, Christopher D.
Tetrahedron, 1999 , vol. 55, # 3 p. 801 - 814
反应条件
1: 90 percent / baker's yeast; sucrose / H2O / 48 h / 23 °C / stirring 2: HN3 / DEAD; TPP / benzene / 72 h / 20 °C View Scheme
参考文献
Afonso; Barros; Godinho; Maycock
Synthesis, 1991 , # 7 p. 575 - 580
参考文献
Warren-Teed Laboratories, Inc.
Patent: US4094988 A1, 1978 ;
反应条件
toluene-4-sulfonic acid in benzene 0.166667 h; Heating;
参考文献
Afonso; Barros; Godinho; Maycock
Synthesis, 1991 , # 7 p. 575 - 580
反应条件
1: 85 percent / Br2, Et3N / CCl4 / 10 h / Ambient temperature 2: 92 percent / H2O, p-toluenesulfonic acid / acetone View Scheme
参考文献
Fjeldskaar, Inger Reidun; Skatteboel, Lars
Acta Chemica Scandinavica, 1991 , vol. 45, # 4 p. 410 - 417
