5-氨基-2-甲氧基苯甲酸甲酯合成路线 （共 13 条）
反应条件
1: 5-amino-2-methoxybenzoic acid methyl ester With hydrogenchloride in water T=0°C; 0.0833333 h; Inert atmosphereSchlenk technique; 2: With tert.-butylnitrite T=0°C; 0.25 h; Inert atmosphereSchlenk technique; 3: trifluoromethylsilver T=-78 - 20°C; 4 h; Inert atmosphereSchlenk technique;
参考文献
Journal of the American Chemical Society, , vol. 135, # 28 p. 10330 - 10333
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in chloroform
T=20°C; 1 h;
参考文献
Zhu, Jiang; Lin, Jian-Bin; Xu, Yun-Xiang; Shao, Xue-Bin; Jiang, Xi-Kui; Li, Zhan-Ting
Journal of the American Chemical Society, 2006 , vol. 128, # 37 p. 12307 - 12313
反应条件
N-ethyl-N,N-diisopropylamine in dichloromethane
参考文献
Aventis Pharmaceuticals Inc.
Patent: US6423704 B1, 2002 ;
US 6423704 B2
Title/Abstract Full Text Show Details
Aventis Pharmaceuticals Inc.
Patent: US6211199 B1, 2001 ;
US 6211199 B1
