3,3’4,4’-联苯四羧酸合成路线 （共 15 条）
反应条件
hydrogenchloride; sodium hydroxide; hydroxylammonium sulfate; palladium in nitrogen; water
反应条件
hydrogenchloride; potassium hydroxide; sodium formate; metallic palladium (Pd)-carbon; Pd-C in ethanol; water
反应条件
hydrogenchloride in water
参考文献
US2013/197261 A1, ;
Paragraph 0100; 0101 ;
反应条件
hydrogenchloride in water
反应条件
1: [Co(O2CCH3)2]*4H2O; Mn(CH3COO)2*4H2O; 2-hydroxy-1,3-isoindolinedione; acetic acid / 5 h / 150 °C / 22502.3 Torr / |Autoclave 2: hydrogenchloride / water View Scheme
反应条件
1: potassium carbonate; bis-triphenylphosphine-palladium(II) chloride / methanol; toluene / 4 h / 80 °C / |Inert atmosphere 2: [Co(O2CCH3)2]*4H2O; Mn(CH3COO)2*4H2O; 2-hydroxy-1,3-isoindolinedione; acetic acid / 5 h / 150 °C / 22502.3 Torr / |Autoclave 3: hydrogenchloride / water View Scheme
反应条件
1: water / 2 h / 100 °C 2: hydrogenchloride / water View Scheme
反应条件
1: palladium 10 on activated carbon / 6 h / 250 °C / |Inert atmosphere 2: [Co(O2CCH3)2]*4H2O; Mn(CH3COO)2*4H2O; 2-hydroxy-1,3-isoindolinedione; acetic acid / 5 h / 150 °C / 22502.3 Torr / |Autoclave 3: hydrogenchloride / water View Scheme
反应条件
1: lanthanum-deposited zeolite / 2 h / 180 °C / |Autoclave; |Inert atmosphere 2: palladium 10 on activated carbon / 6 h / 250 °C / |Inert atmosphere 3: [Co(O2CCH3)2]*4H2O; Mn(CH3COO)2*4H2O; 2-hydroxy-1,3-isoindolinedione; acetic acid / 5 h / 150 °C / 22502.3 Torr / |Autoclave 4: hydrogenchloride / water View Scheme
反应条件
potassium permanganate
参考文献
Chemische Berichte, , vol. 26, p. 2486
