4-氯-N,N-二甲基丁酰胺合成路线 （共 6 条）
反应条件
dimethyl amine in tetrahydrofuran
反应条件
sodium hydroxide; 1,2-dichloro-ethane
参考文献
Journal of the American Chemical Society, , vol. 78, p. 6123,6124
反应条件
in benzene 12 h; Heating;
参考文献
Levin, Jeremy I.; Turos, Edward; Weinreb, Steven M.
Synthetic Communications, 1982 , vol. 12, # 13 p. 989 - 994
反应条件
in diethyl ether T=0°C; 1 h;
参考文献
Organic Magnetic Resonance, , vol. 14, # 5 p. 349 - 355
反应条件
1: 75.4 percent / methanol
2: 46.8 percent / LiAlH4 / diethyl ether / Heating
3: 1) NH2-CS-NH2, aq. HBr, 2) aq. NaOH (10percent) / 1) reflux, 2) reflux
View Scheme
参考文献
Uneme, Hideki; Mitsudera, Hiroyuki; Kamikado, Toshiya; Kono, Yoshiaki; Manabe, Yukiaki; Numata, Mitsuo
Bioscience, Biotechnology, and Biochemistry, 1992 , vol. 56, # 12 p. 2023 - 2033
