2-(4-氯苯基)-5-甲基-1,3,4-噁二唑合成路线 (共 4 条)
反应条件
in ethylene glycol dimethyl ether T=220°C; Huisgen reaction; P=8250.83 - 10501.1 Torr; 0.0833333 h; Microwave irradiationSealed vial;
参考文献
Reichart, Benedikt; Kappe, C. Oliver
Tetrahedron Letters, 2012 , vol. 53, # 8 p. 952 - 955
反应条件
1: With iodine; caesium carbonate in dimethyl sulfoxide T=20°C; Green chemistry; 2: With dihydrogen peroxide in water; dimethyl sulfoxide T=20°C; 9 h; Green chemistry;
参考文献
Majji, Ganesh; Rout, Saroj Kumar; Guin, Srimanta; Gogoi, Anupal; Patel, Bhisma K.
RSC Advances, 2014 , vol. 4, # 11 p. 5357 - 5362
反应条件
sulfuric acid; silica gel T=20°C;
参考文献
Dabiri, Minoo; Salehi, Peyman; Baghbanzadeh, Mostafa; Zolfigol, Mohammad Ali; Bahramnejad, Mahboobeh
Synthetic Communications, 2007 , vol. 37, # 7 p. 1201 - 1209
反应条件
trifluorormethanesulfonic acid; dimethyl-dichlorosilane in acetonitrile T=80°C; 24 h;
参考文献
Rigo, Benoit; Cauliez, Pascal
Synthetic Communications, 1988 , vol. 18, # 11 p. 1247 - 1252