D(-)-对羟基苯甘氨酸合成路线 （共 36 条）
反应条件
20 wt. Pd(OH)2 on activated carbon; hydrogen; trifluoroacetic acid in water T=20°C; P=3040.2 Torr; 24 h;
参考文献
Liu, Chaomin; Molinski, Tadeusz F.
Chemistry - An Asian Journal, 2011 , vol. 6, # 8 p. 2022 - 2027
反应条件
hydrogenchloride; water T=50°C; 10 h;
参考文献
Grundmann, Peter; Fessner, Wolf-Dieter
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 11-12 p. 1729 - 1735
反应条件
hydrogenchloride; C15H13O4S(1-)*K(1+); C15H12ClO4S(1-)*K(1+) in water; isopropyl alcohol Resolution of racemate;
参考文献
US6639103 B1, ;
Page/Page column 12-13 ;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 65, # 4 p. 965 - 970
Synthetic Communications, , vol. 24, # 17 p. 2449 - 2459
反应条件
aminoacylase I from Aspergillus melleus; Tris buffer in water T=25°C; pH=6.5; 5 h; Title compound not separated from byproducts;
参考文献
Tetrahedron Asymmetry, , vol. 15, # 12 p. 1933 - 1936
反应条件
in water T=30°C; 48 h; 0.1 M potassium phosphate buffer (pH = 8.0); cells of Pseudomonas sp. AJ-11220 (bacterioal strain H-231); ivestigate steric configuration of the product; other time;
参考文献
Yokozeki, Kenzo; Nakamori, Shigeru; Eguchi, Chikahiko; Yamada, Kazuhiko; Mitsugi, Koji
Agricultural and Biological Chemistry, 1987 , vol. 51, # 2 p. 355 - 362
反应条件
1: selenium(IV) oxide / ethyl acetate / 1 h / 75 °C 2: platinum(IV) oxide; hydrogen / 3040.2 Torr 3: 20 wt. Pd(OH)2 on activated carbon; hydrogen; trifluoroacetic acid / water / 24 h / 20 °C / 3040.2 Torr 4: hydrogenchloride; water / 24 h / 90 - 100 °C View Scheme
参考文献
Chemistry - An Asian Journal, , vol. 6, # 8 p. 2022 - 2027
反应条件
1: platinum(IV) oxide; hydrogen / 3040.2 Torr 2: 20 wt. Pd(OH)2 on activated carbon; hydrogen; trifluoroacetic acid / water / 24 h / 20 °C / 3040.2 Torr 3: hydrogenchloride; water / 24 h / 90 - 100 °C View Scheme
参考文献
Chemistry - An Asian Journal, , vol. 6, # 8 p. 2022 - 2027
反应条件
1: 20 wt. Pd(OH)2 on activated carbon; hydrogen; trifluoroacetic acid / water / 24 h / 20 °C / 3040.2 Torr 2: hydrogenchloride; water / 24 h / 90 - 100 °C View Scheme
参考文献
Chemistry - An Asian Journal, , vol. 6, # 8 p. 2022 - 2027
反应条件
1.1: diethylamino-sulfur trifluoride / dichloromethane / 1.25 h / -78 °C 1.2: 4 h / -78 - 20 °C 2.1: selenium(IV) oxide / ethyl acetate / 1 h / 75 °C 3.1: platinum(IV) oxide; hydrogen / 3040.2 Torr 4.1: 20 wt. Pd(OH)2 on activated carbon; hydrogen; trifluoroacetic acid / water / 24 h / 20 °C / 3040.2 Torr 5.1: hydrogenchloride; water / 24 h / 90 - 100 °C View Scheme
参考文献
Chemistry - An Asian Journal, , vol. 6, # 8 p. 2022 - 2027
