4-甲氧基苯基 异硫氰酸酯合成路线 （共 89 条）
反应条件
sodium hydroxide in dichloromethane T=0 - 20°C; 6 h;
参考文献
Li, Zheng-Yi; Ma, Hong-Zhao; Han, Chen; Xi, Hai-Tao; Meng, Qi; Chen, Xin; Sun, Xiao-Qiang
Synthesis (Germany), 2013 , vol. 45, # 12 art. no. SS-2013-F0228-OP, p. 1667 - 1674
反应条件
1: 4-Methoxyphenylazide With triphenylphosphine in chloroform T=20°C; 1.5 h; 2: carbon disulfide in chloroform T=20°C; aza-Wittig reaction; 1 h;
参考文献
Isoda, Takeshi; Hayashi, Kazuhiko; Tamai, Satoshi; Kumagai, Toshio; Nagao, Yoshimitsu
Chemical and Pharmaceutical Bulletin, 2006 , vol. 54, # 11 p. 1616 - 1619
反应条件
1: tetrahydrofuran / 1.5 h / 22 °C 2: 97 percent / tosyl chloride / tetrahydrofuran / 1 h / 0 - 22 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 72, # 10 p. 3969 - 3971
反应条件
sodium hydroxide in toluene 1.5 h; Heating;
参考文献
Chawng Siek Pak; In Kwon Youn; Yeon Soo Lee
Synthesis, 1982 , # 11 p. 969 - 970
反应条件
1,1'-(ethane-1,2-diyl)dipyridinium ditribromide; triethylamine in acetonitrile Cooling with ice;
参考文献
Yella, Ramesh; Ghosh, Harisadhan; Murru, Siva; Sahoo, Santosh K.; Patel, Bhisma K.
Synthetic Communications, 2010 , vol. 40, # 14 p. 2083 - 2096
反应条件
Cu(BF4)2*6H2O in hexadeuterioacetone; water T=-10°C; Meerwein Arylation; 2.5 h;
参考文献
Baranovskii; Petrushka; Fesak; Grishchuk
Russian Journal of General Chemistry, 2013 , vol. 83, # 2 p. 325 - 328
Zh. Obshch. Khim., 2013 , vol. 83, # 2 p. 271 - 274,4
反应条件
iron(II) bis(thiocyanate) in water; acetone T=-40 - -20°C;
参考文献
Grishchuk, B. D.; Gorbovoi, P. M.; Ganushchak, N. I.; Brush, D. M.; Kudrik, E. Ya.
Russian Journal of General Chemistry, 1993 , vol. 63, # 7.2 p. 1156 - 1158
Zhurnal Obshchei Khimii, 1993 , vol. 63, # 7 p. 1655 - 1658
反应条件
copper diacetate in water; acetone T=-40 - -30°C;
参考文献
Gorbovoi; Zagrichuk; Grichshuk
Russian Journal of General Chemistry, 2000 , vol. 70, # 5 p. 755 - 757
反应条件
triethylamine in chloroform 1 h; Ambient temperature;
参考文献
Fueloep, Vilmos; Kalman, Alajos; Beckert, Rainer; Fabian, Juergen
Monatshefte fuer Chemie, 1989 , vol. 120, p. 561 - 570
反应条件
1,1,2-trichloroethylene; Cu(SCN)2 in water; acetone T=-25 - -20°C; 1.5 h;
参考文献
Grishchuk, B. D.; Kudrik, E. Ya.; Gorbovoi, P. M.; Garmider, V. L.; Ganushchak, N. I.
Russian Journal of General Chemistry, 1994 , vol. 64, # 8.1 p. 1164 - 1166
Zhurnal Obshchei Khimii, 1994 , vol. 64, # 8 p. 1294 - 1297
