4-甲氧基苯基 异硫氰酸酯合成路线 (共 89 条)
反应条件
(i) aq. Me3N, (ii) Ac2O; Multistep reaction;
参考文献
Garraway,J.L.
Journal of the Chemical Society, 1961 , p. 3733 - 3735
参考文献
Biswas, Kallolmay; Greaney, Michael F.
Organic Letters, 2011 , vol. 13, # 18 p. 4946 - 4949
反应条件
1.1: Et3N / dimethylformamide / 0.5 h / 20 °C 1.2: dimethylformamide / 40 - 45 °C 2.1: dimethylformamide / 20 °C 3.1: 60 percent / 250 - 260 °C View Scheme
参考文献
Tang, Jing; Huang, Xian
Journal of Chemical Research - Part S, 2003 , # 3 p. 140 - 141
反应条件
iron; paraffin oil T=280 - 290°C;
参考文献
Bayer and Co.
Patent: DE259364 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 11, p. 205
Full Text Show Details
Salkowski
Chemische Berichte, 1874 , vol. 7, p. 1012
反应条件
in acetonitrile
T=25°C; 0.166667 h; Milling;
参考文献
Strukil, Vjekoslav; Igrc, Marina D.; Fabian, Laszlo; Eckert-Maksic, Mirjana; Childs, Scott L.; Reid, David G.; Duer, Melinda J.; Halasz, Ivan; Mottillo, Cristina; Friscic, Tomislav
Green Chemistry, 2012 , vol. 14, # 9 p. 2462 - 2473
反应条件
mercury(II) diacetate; triethylamine in 1,4-dioxane
T=20°C;
参考文献
Singh, Okram Mukherjee; Singh, Sarangthem Joychandra
Journal of Chemical Research, 2006 , # 8 p. 483 - 485
参考文献
Mayekar, Amita V.; Bobade, Anil S.; Patil; Athlekar; Chowdhary, Abhay S.
Indian Journal of Heterocyclic Chemistry, 2010 , vol. 19, # 3 p. 297 - 298
反应条件
aluminium trichloride
参考文献
Gattermann
Journal fuer Praktische Chemie (Leipzig), 1899 , vol. <2>59, p. 589
反应条件
1: benzene / 5 h / Heating
2: 76 percent / NaOH / ethanol; H2O / 5 h / Heating
View Scheme
参考文献
Misra; Sen Gupta
Pharmazie, 1982 , vol. 37, # 4 p. 254 - 256
反应条件
in ethanol
2 h; Heating;
参考文献
Pandey, A. K.; Singh, R.; Verma, V. K.
Acta Chimica Hungarica, 1983 , vol. 114, # 2 p. 107 - 112