(9CI)-4-(3-吡啶氧基)-丁醛合成路线 （共 5 条）
反应条件
sodium hypochlorite; water; sodium hydrogencarbonate; 4-methoxy-2,2,6,6-tetramethylpiperidine-1-oxy; sodium chloride; potassium bromide in dichloromethane T=0°C; 0.5 h;
参考文献
Bach, Andrew T.; Carlson, John A.; Giannousis, Peter P.
Synthesis, 1999 , # 5 p. 769 - 774
反应条件
hydrogenchloride; water T=60 - 65°C; 2 h;
参考文献
Bach, Andrew T.; Carlson, John A.; Giannousis, Peter P.
Synthesis, 1999 , # 5 p. 769 - 774
反应条件
1: 86 percent / potassium t-amylate / toluene; dimethylformamide / 2 h / 100 °C 2: 94 percent / HCl, H2O / 2 h / 60 - 65 °C View Scheme
参考文献
Bach, Andrew T.; Carlson, John A.; Giannousis, Peter P.
Synthesis, 1999 , # 5 p. 769 - 774
反应条件
1: 99 percent / NaOH, H2O / methanol / 0.75 h / 25 °C 2: 91 percent / NaOCl, 4-MeO-TEMPO, NaHCO3, NaCl, KBr, H2O / CH2Cl2 / 0.5 h / 0 °C View Scheme
参考文献
Bach, Andrew T.; Carlson, John A.; Giannousis, Peter P.
Synthesis, 1999 , # 5 p. 769 - 774
反应条件
1: 99 percent / HCl, H20 / methanol / 1 h / 5 °C 2: 91 percent / NaOH, 4-MeO-TEMPO, NaOCl, H2O, NaHCO3, KBr / CH2Cl2; H2O / 0.5 h / 0 °C View Scheme
参考文献
Bach, Andrew T.; Carlson, John A.; Giannousis, Peter P.
Synthesis, 1999 , # 5 p. 769 - 774
