4-[(4-硝基苯基)硫代]甲苯合成路线 （共 45 条）
反应条件
sulfur in N,N-dimethyl acetamide
electrolyse, catholyte N(Et)4ClO4; Yield given;
参考文献
Robert, Julie; Anouti, Meriem; Bosser, Gerard; Parrain, Jean-Luc; Paris, Jacky
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1995 , # 8 p. 1639 - 1644
反应条件
aluminum tri-bromide; mercury(II) diacetate in dichloromethane
T=-20°C; 5 h; Yield given. Yields of byproduct given;
参考文献
Zefirov, N. S.; Zyk, N. V.; Beloglazkina, E. K.; Tyurin, V. S.
Russian Chemical Bulletin, 1995 , vol. 44, # 2 p. 315 - 317
Izvestiya Akademi Nauk, Seriya Khimicheskaya, 1995 , # 2 p. 324 - 326
反应条件
1: copper(l) iodide; Na2S*9H2O; sulfur / N,N-dimethyl-formamide / 15 h / 110 °C / Inert atmosphere
2: iron; potassium carbonate / dimethyl sulfoxide; N,N-dimethyl-formamide / 18 h / 120 °C / Inert atmosphere
View Scheme
参考文献
Li, Yaming; Nie, Caiping; Wang, Huifeng; Li, Xiaoying; Verpoort, Francis; Duan, Chunying
European Journal of Organic Chemistry, 2011 , # 36 p. 7331 - 7338
反应条件
sulfur; para-dinitrobenzene in N,N-dimethyl acetamide
electrolyse, catholyte N(Et)4ClO4; Further byproducts given;
参考文献
Robert, Julie; Anouti, Meriem; Bosser, Gerard; Parrain, Jean-Luc; Paris, Jacky
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1995 , # 8 p. 1639 - 1644
反应条件
sodium hydride in N,N,N',N',N'',N''-hexamethylphosphoric triamide
2 h;
参考文献
Baum, James Clayton; Bolhassan, Jimat; Langler, Richard Francis; Pujol, Paul Joseph; Raheja, Raj Kumar
Canadian Journal of Chemistry, 1990 , vol. 68, # 8 p. 1450 - 1455
反应条件
1: 56 percent / triethylamine / pyridine
2: sodium hydride / hexamethylphosphoric acid triamide / 2 h
View Scheme
参考文献
Baum, James Clayton; Bolhassan, Jimat; Langler, Richard Francis; Pujol, Paul Joseph; Raheja, Raj Kumar
Canadian Journal of Chemistry, 1990 , vol. 68, # 8 p. 1450 - 1455
反应条件
1: 46 percent / triethylamine / pyridine
2: sodium hydride / hexamethylphosphoric acid triamide / 2 h / Ambient temperature
View Scheme
参考文献
Baum, James Clayton; Bolhassan, Jimat; Langler, Richard Francis; Pujol, Paul Joseph; Raheja, Raj Kumar
Canadian Journal of Chemistry, 1990 , vol. 68, # 8 p. 1450 - 1455
反应条件
ethanol; sodium hydride in N,N,N',N',N'',N''-hexamethylphosphoric triamide
Yields of byproduct given;
参考文献
Durkin, Kathleen Anne; Langler, Richard Francis; Morrison Nancy Ann
Canadian Journal of Chemistry, 1988 , vol. 66, p. 3070 - 3076
反应条件
sodium hydride in N,N,N',N',N'',N''-hexamethylphosphoric triamide
2 h; Ambient temperature;
参考文献
Baum, James Clayton; Bolhassan, Jimat; Langler, Richard Francis; Pujol, Paul Joseph; Raheja, Raj Kumar
Canadian Journal of Chemistry, 1990 , vol. 68, # 8 p. 1450 - 1455
反应条件
sodium hydride in N,N,N',N',N'',N''-hexamethylphosphoric triamide
2 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Baum, James Clayton; Bolhassan, Jimat; Langler, Richard Francis; Pujol, Paul Joseph; Raheja, Raj Kumar
Canadian Journal of Chemistry, 1990 , vol. 68, # 8 p. 1450 - 1455
