4-[(4-硝基苯基)硫代]甲苯合成路线 （共 45 条）
反应条件
sulfur trioxide
1.) CH2Cl2, -70 deg C, 15 min, 2.) -30 deg C, 1 h; -30 deg C -> 20 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Zefirov, N. S.; Zyk, N. V.; Beloglazkina, E. K.; Tyurin, V. S.
Russian Chemical Bulletin, 1995 , vol. 44, # 2 p. 315 - 317
Izvestiya Akademi Nauk, Seriya Khimicheskaya, 1995 , # 2 p. 324 - 326
参考文献
Chandrasekaran, R.; Perumal, S.; Wilson, D.A.
Magnetic Resonance in Chemistry, 1987 , vol. 25, p. 1001 - 1006
反应条件
in N,N-dimethyl-formamide
T=-10 - 20°C; Kinetics;
参考文献
Beltrame,P.; Carniti,P.
Gazzetta Chimica Italiana, 1973 , vol. 103, p. 723 - 730
反应条件
1: hydrogen peroxide / acetic acid
2: 66 percent / S8, liq. NH3 / 6 h / 20 °C / other 4-nitrophenyl substituted phenyl sulfoxides, other arenesulfonamides
View Scheme
参考文献
Sato, Ryu; Chiba, Shuji; Takikawa, Yuji; Takizawa, Saburo; Saito, Minoru
Chemistry Letters, 1983 , p. 535 - 538
反应条件
peroxymonosulfuric acid; silica gel in acetonitrile
6.5 h; Heating;
参考文献
Lakouraj, Moslem M.; Movassagh; Ghodrati
Synthetic Communications, 2002 , vol. 32, # 6 p. 847 - 850
