2-(3-氯苯基)苯并[d]噻唑合成路线 (共 22 条)
反应条件
silica gel; carbon; toluene-4-sulfonic acid
0.133333 h; microwave irradiation;
参考文献
Rostamizadeh, Shahnaz; Housaini
Phosphorus, Sulfur and Silicon and the Related Elements, 2005 , vol. 180, # 5-6 p. 1321 - 1326
反应条件
1-propanephosphonic acid cyclic anhydride; N-ethyl-N,N-diisopropylamine in ethyl acetate
T=100°C; 0.166667 h; Microwave irradiationSealed tube;
参考文献
Wen, Xiaoan; Bakali, Jamal El; Deprez-Poulain, Rebecca; Deprez, Benoit
Tetrahedron Letters, 2012 , vol. 53, # 19 p. 2440 - 2443
反应条件
dimethyl sulfoxide; 1-propanephosphonic acid cyclic anhydride in ethyl acetate
T=0 - 25°C; 2 h; Inert atmosphere; chemoselective reaction;
参考文献
Raghavendra, Goravanahalli M.; Ramesha, Ajjahalli B.; Revanna, Cigalli N.; Nandeesh, Kebbahalli N.; Mantelingu, Kempegowda; Rangappa, Kanchugarakoppal S.
Tetrahedron Letters, 2011 , vol. 52, # 43 p. 5571 - 5574
反应条件
anhydrous iron chloride; Cu(OAc)2*2H2O; palladium dichloride in N,N-dimethyl-formamide
T=120°C; 24 h;
参考文献
Wu, Xiang-Mei; Shen, Qiu-Xian
Letters in Organic Chemistry, 2013 , vol. 10, # 9 p. 668 - 673
反应条件
1,4-diaza-bicyclo[2.2.2]octane; 1,10-phenanthroline; copper (II) acetate monohydrate; sulfur in dimethyl sulfoxide
T=100°C;
参考文献
Wang, Rui; Ding, Yong-Liang; Liu, Hong; Peng, Shu; Ren, Jie; Li, Lei
Tetrahedron Letters, 2014 , vol. 55, # 4 p. 945 - 949
反应条件
tert.-butylhydroperoxide; copper dichloride in water
T=80°C; 24.5 h; Inert atmosphereSchlenk technique;
参考文献
Zhang, Mingliang; Lu, Wen-Ting; Ruan, Wenqing; Zhang, Hui-Jun; Wen, Ting-Bin
Tetrahedron Letters, 2014 , vol. 55, # 10 p. 1806 - 1809
反应条件
in neat (no solvent)
1 h; Green chemistry; Time;
参考文献
Yoon, Soon Byung; Chun, Eun Jeong; Noh, Young Ri; Yoon, Yong Jin; Lee, Sang-Geyong
Bulletin of the Korean Chemical Society, 2013 , vol. 34, # 9 p. 2819 - 2821
反应条件
oxygen; copper(II) sulfate in dimethyl sulfoxide
T=130°C; 44 h; Sealed tube;
参考文献
Song, Qiuling; Feng, Qiang; Zhou, Mingxin
Organic Letters, 2013 , vol. 15, # 23 p. 5990 - 5993
反应条件
(R)-(+)-1,1'-binaphthyl-2,2'-diamine; caesium carbonate; copper dichloride in acetonitrile
T=110°C; 36 h; Inert atmosphere;
参考文献
Jaseer; Prasad; Dandapat, Arpan; Sekar, Govindasamy
Tetrahedron Letters, 2010 , vol. 51, # 38 p. 5009 - 5012
反应条件
dipotassium peroxodisulfate in water; dimethyl sulfoxide
T=100°C; 3 h; Inert atmosphere;
参考文献
Yang, Zhiyong; Chen, Xiang; Wang, Sizhuo; Liu, Jidan; Xie, Kai; Wang, Anwei; Tan, Ze
Journal of Organic Chemistry, 2012 , vol. 77, # 16 p. 7086 - 7091