1-(2,4-双(苄氧基)苯基)乙酮合成路线 （共 22 条）
反应条件
potassium carbonate in acetonitrile 48 h; Heating / reflux;
参考文献
Qian, Changgeng; Cai, Xiong; Zhai, Haixiao
Patent: US2009/76006 A1, 2009 ;
Location in patent: Page/Page column 32; 41 ;
US 20090076006 A1
反应条件
18-crown-6 ether; potassium carbonate; potassium iodide in acetone 16 h; Inert atmosphereReflux;
参考文献
Acuna, A. Ulises; Amat-Guerri, Francisco; Morcillo, Purificacion; Liras, Marta; Rodriguez, Benjamin
Organic Letters, 2009 , vol. 11, # 14 p. 3020 - 3023
反应条件
potassium carbonate in acetone Heating;
参考文献
Dewick, Paul M.
Synthetic Communications, 1981 , vol. 11, # 10 p. 853 - 858
反应条件
in tetrahydrofuran; hexane; mineral oil
参考文献
Glaxo Inc.
Patent: US5126351 A1, 1992 ;
参考文献
Mullaji; Shah
Proceedings - Indian Academy of Sciences, Section A, 1951 , vol. 34, p. 88,94
反应条件
1: 92.1 percent / 50percent aq. KOH / ethanol / 24 h / Ambient temperature 2: thallium nitrate / CHCl3 / Ambient temperature 3: H2, triethylamine / 10percent Pd/C / ethyl acetate / 760 Torr / Ambient temperature 4: 5percent HCl / methanol / 2 h / Heating View Scheme
参考文献
Nishiyama, Kiyotoshi; Esaki, Sachiko; Deguchi, Ikuko; Sugiyama, Naoko; Kamiya, Shintaro
Bioscience, Biotechnology, and Biochemistry, 1993 , vol. 57, # 1 p. 107 - 114
反应条件
1: potassium hydroxide / ethanol; water / 0 - 20 °C 2: boron trichloride / dichloromethane / 0.5 h / Cooling with ice View Scheme
参考文献
Ma, Lei; Yang, Zhengyi; Li, Chenjing; Zhu, Zhiyuan; Shen, Xu; Hu, Lihong
Journal of Enzyme Inhibition and Medicinal Chemistry, 2011 , vol. 26, # 5 p. 643 - 648
反应条件
1: potassium hydroxide / ethanol; water / 0 - 20 °C 2: boron trichloride / dichloromethane / 0.5 h / Cooling with ice View Scheme
参考文献
Ma, Lei; Yang, Zhengyi; Li, Chenjing; Zhu, Zhiyuan; Shen, Xu; Hu, Lihong
Journal of Enzyme Inhibition and Medicinal Chemistry, 2011 , vol. 26, # 5 p. 643 - 648
反应条件
1: potassium hydroxide / ethanol; water / 0 - 20 °C 2: boron trichloride / dichloromethane / 0.5 h / Cooling with ice View Scheme
参考文献
Ma, Lei; Yang, Zhengyi; Li, Chenjing; Zhu, Zhiyuan; Shen, Xu; Hu, Lihong
Journal of Enzyme Inhibition and Medicinal Chemistry, 2011 , vol. 26, # 5 p. 643 - 648
反应条件
1: 80.5 percent / 50percent aq. KOH / ethanol / 24 h / Ambient temperature 2: thallium nitrate / CHCl3 / Ambient temperature 3: H2, triethylamine / 10percent Pd/C / ethyl acetate / 760 Torr / Ambient temperature 4: 5percent HCl / methanol / 2 h / Heating View Scheme
参考文献
Nishiyama, Kiyotoshi; Esaki, Sachiko; Deguchi, Ikuko; Sugiyama, Naoko; Kamiya, Shintaro
Bioscience, Biotechnology, and Biochemistry, 1993 , vol. 57, # 1 p. 107 - 114
