1-(2,4-双(苄氧基)苯基)乙酮合成路线 （共 22 条）
反应条件
1: 89 percent / silver trifluoroacetate, iodine / CHCl3 / 1 h / 20 - 25 °C
2: 1.) BBr3; 2.) water / 1.) CH2Cl2, -70 deg C, 5 min; 2.) 1 h
3: 85 percent / K2CO3 / acetone / 0.75 h / Heating
4: 97 percent / PPh3, CuI / PdCl2 / triethylamine; dimethylformamide / 0.8 h / 80 °C
5: 88 percent / K2CO3 / methanol / 0.8 h / Heating
6: 82 percent / BBr3 / CH2Cl2 / 0.08 h / -70 °C
View Scheme
参考文献
Sogawa, Akihiro; Tsukayama, Masao; Nozaki, Hiroshi; Nakayama, Mitsuru
Heterocycles, 1996 , vol. 43, # 1 p. 101 - 111
反应条件
1: 89 percent / silver trifluoroacetate, iodine / CHCl3 / 1 h / 20 - 25 °C
2: 1.) BBr3; 2.) water / 1.) CH2Cl2, -70 deg C, 5 min; 2.) 1 h
View Scheme
参考文献
Sogawa, Akihiro; Tsukayama, Masao; Nozaki, Hiroshi; Nakayama, Mitsuru
Heterocycles, 1996 , vol. 43, # 1 p. 101 - 111
