1-甲基-2,8,9-三氧杂-5-氮杂-1-硅杂二环[3.3.3]十一烷合成路线 （共 23 条）
反应条件
disodium hydrogenphosphate; potassium dihydrogenphosphate T=40 - 70°C; hydrolysis in neutral medium; KineticsThermodynamic dataMechanism;
参考文献
Voronkov, M. G.; Toryashinova, D-S. D.; Baryshok, V. P.; Shainyan, B. A.; Brodskaya, E. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, # 12 p. 2447 - 2450
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 12 p. 2673 - 2676
反应条件
disodium hydrogenphosphate; potassium dihydrogenphosphate T=40 - 70°C; hydrolysis in neutral medium; KineticsThermodynamic dataMechanism;
参考文献
Voronkov, M. G.; Toryashinova, D-S. D.; Baryshok, V. P.; Shainyan, B. A.; Brodskaya, E. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, # 12 p. 2447 - 2450
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 12 p. 2673 - 2676
反应条件
iodine cloride in dichloromethane T=20°C; Chlorination;
参考文献
Voronkov; Baryshok; Lazareva
Russian Chemical Bulletin, 1996 , vol. 45, # 8 p. 1970 - 1972
反应条件
bromine in dichloromethane T=-5°C; Bromination;
参考文献
Voronkov; Baryshok; Lazareva
Russian Chemical Bulletin, 1996 , vol. 45, # 8 p. 1970 - 1972
反应条件
in hexadeuterioacetone Kinetics; byproducts: ClSi(OCH2CH2)3N; not isolated, reaction followed by (1)H-NMR spectroscopy;
参考文献
Journal of Organometallic Chemistry, , vol. 296, p. 315 - 320
反应条件
in hexadeuterioacetone Kinetics; byproducts: ISi(OCH2CH2)3N; not isolated, reaction followed by (1)H-NMR spectroscopy;
参考文献
Nies, J. Dirk; Bellama, Jon M.; Ben-Zvi, Nava
Journal of Organometallic Chemistry, 1985 , vol. 296, p. 315 - 320
反应条件
in benzene 3 h; Heating;
参考文献
European Journal of Medicinal Chemistry, , vol. 24, # 1 p. 48 - 54
反应条件
potassium hydroxide in 1,4-dioxane
T=80°C; 1 h;
参考文献
D'yakov, V. M.; Makarov, A. F.
J. Gen. Chem. USSR (Engl. Transl.), 1992 , vol. 62, # 2.2 p. 359 - 363,291 - 294
反应条件
sodium ethanolate in N,N-dimethyl-formamide
T=140°C; 22 h;
参考文献
Gevorgyan, Vladimir; Borisova, Larisa; Vyater, Armand; Ryabova, Victoria; Lukevics, Edmunds
Journal of Organometallic Chemistry, 1997 , vol. 548, # 2 p. 149 - 155
反应条件
sodium isopropanolate in isopropyl alcohol
20 h;
参考文献
D'yakov, V. M.; Makarov, A. F.
J. Gen. Chem. USSR (Engl. Transl.), 1992 , vol. 62, # 2.2 p. 359 - 363,291 - 294
