4-氨基-3,5-二氯吡啶合成路线 （共 19 条）
反应条件
1: With hydrogenchloride; dihydrogen peroxide in water T=10 - 72°C; 3.25 h; 2: With sodium hydroxide in water T=45°C; pH=9 - 10; 0.5 h; Reagent/catalystTemperature;
参考文献
Cook, David C.; Jones, Ronald H.; Kabir, Humayun; Lythgoe, David J.; McFarlane, Ian M.; Pemberton, Clive; Thatcher, Alan A.; Thompson, David M.; Walton, John B.
Organic Process Research and Development, 1998 , vol. 2, # 3 p. 157 - 168
反应条件
lithium amide in ammonia 0 deg C to RT;
参考文献
De Munno, Angela; Bertini, Vincenzo; Picci, Nevio; Lemma, Francesca; Pocci, Marco
Heterocycles, 1998 , vol. 48, # 6 p. 1203 - 1211
反应条件
ammonium hydroxide T=150°C; im Rohr;
参考文献
Journal of the Chemical Society, , vol. 99, p. 1682
反应条件
hydrogenchloride; dihydrogen peroxide
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 69, p. 673,690
反应条件
1: sodium nitrite; copper-powder; aqueous hydrochloric acid / Diazotization 2: aqueous NH3 / 190 °C 3: concentrated aqueous HCl; aqueous H2O2 View Scheme
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 69, p. 673,690
反应条件
1: aqueous NH3 / 190 °C 2: concentrated aqueous HCl; aqueous H2O2 View Scheme
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 69, p. 673,690
参考文献
Journal of the Chemical Society, , vol. 99, p. 1682
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 69, p. 673,690
反应条件
Erhitzen ueber den Schmelzpunkt;
参考文献
Journal of the Chemical Society, , vol. 99, p. 1682
