1: With potassium carbonate in N,N-dimethyl-formamide T=20°C; 2: With hydrogenchloride in ethyl acetate T=20°C; 3: With acetic acid in 1,4-dioxane Heating / reflux;
1: 59 percent 2: 89 percent / toluene / 22 h / Heating 3: 75 percent / 0.417 M nitrosyl chloride, triethylamine / CCl4; tetrahydrofuran / 14 h / Ambient temperature 4: hydrolysis View Scheme
参考文献
Hickey, Deirdre M. B.; MacKenzie, A. Roderick; Moody, Christopher J.; Rees, Charles W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 921 - 926
Hickey, Deirdre M. B.; MacKenzie, A. Roderick; Moody, Christopher J.; Rees, Charles W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 921 - 926