4-甲氧基二甲基邻苯二甲酯合成路线 （共 13 条）
反应条件
1: With potassium hydroxide; water in methanol 4 h; Heating / reflux; 2: With hydrogenchloride in water pH=<= 2;
参考文献
WO2008/44029 A1, ;
Page/Page column 203 ;
反应条件
1: sodium hydroxide / acetone / 6 h / 20 °C / |Inert atmosphere 2: acetic anhydride / 21 h / |Inert atmosphere; |Reflux View Scheme
参考文献
De Nanteuil, Florian; Serrano, Eloisa; Perrotta, Daniele; Waser, Jerome
Journal of the American Chemical Society, 2014 , vol. 136, # 17 p. 6239 - 6242
反应条件
1: 2.8 g / 11 N NaOH / acetone / 25 °C
2: 1) acetic anhydride, 2) urea / 1) reflux, 24h, 2) xylene, reflux, 20h
View Scheme
参考文献
De Nanteuil, Florian; Serrano, Eloisa; Perrotta, Daniele; Waser, Jerome
Journal of the American Chemical Society, 2014 , vol. 136, # 17 p. 6239 - 6242
