6H-苯并[c]苯并吡喃合成路线 （共 63 条）
反应条件
in water; acetonitrile
Irradiation;
参考文献
Huang, C.-G.; Wan, Peter
Journal of Organic Chemistry, 1991 , vol. 56, # 16 p. 4846 - 4853
反应条件
bis-triphenylphosphine-palladium(II) chloride; sodium acetate in N,N-dimethyl acetamide
T=160°C; 2 h;
参考文献
Ames, D.E.; Opalko, A.
Tetrahedron, 1984 , vol. 40, # 10 p. 1919 - 1926
反应条件
1: 92 percent / potassium carbonate / acetone / 50 °C
2: 91 percent / potassium acetate / Pd(OH)2/C / N,N-dimethyl-acetamide / 145 °C
View Scheme
参考文献
Parisien, Mathieu; Valette, Damien; Fagnou, Keith
Journal of Organic Chemistry, 2005 , vol. 70, # 19 p. 7578 - 7584
反应条件
tert-Butyl thionitrate
T=160°C; 0.5 h;
参考文献
Oae, Shigeru; Iida, Kazuyuki; Shinhama, Koichi; Takata, Toshikazu
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 8 p. 2374 - 2378
反应条件
1: K2CO3; NaI / acetone / Heating
2: Pd(OAc)2; PCy3*HBF4; K2CO3 / N,N-dimethyl-acetamide / 130 °C
View Scheme
参考文献
Campeau, Louis-Charles; Parisien, Mathieu; Jean, Annie; Fagnou, Keith
Journal of the American Chemical Society, 2006 , vol. 128, # 2 p. 581 - 590
反应条件
Pd2(PPh3)2Cl2; potassium tert-butylate; triphenylphosphine
1 h; RefluxInert atmosphere; Reagent/catalyst;
参考文献
Ahmed, Atiur; Dhara, Shubhendu; Ray, Jayanta K.
Tetrahedron Letters, 2013 , vol. 54, # 13 p. 1673 - 1676
反应条件
Co(acetylacetonate)3; lithium hexamethyldisilazane
T=80°C; 48 h; Inert atmosphere;
参考文献
Liu, Wei; Cao, Hao; Xin, Jie; Jin, Liqun; Lei, Aiwen
Chemistry - A European Journal, 2011 , vol. 17, # 13 p. 3588 - 3592
反应条件
palladium diacetate; potassium carbonate; triphenylphosphine in 1-methyl-pyrrolidin-2-one
T=150°C; 72 h; Inert atmosphere;
参考文献
Shen, Zengming; Ni, Zhenjie; Mo, Song; Wang, Jing; Zhu, Yamin
Chemistry - A European Journal, 2012 , vol. 18, # 16 p. 4859 - 4865
反应条件
in water
T=60 - 150°C; Microwave irradiation; TemperatureSolventTime;
参考文献
He, Yan; Zhang, Xinying; Cui, Liangyan; Wang, Jianji; Fan, Xuesen
Green Chemistry, 2012 , vol. 14, # 12 p. 3429 - 3435
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in toluene
T=80°C;
参考文献
Harrowven, David C.; Nunn, Michael I.T.; Newman, Nicola A.; Fenwick, David R.
Tetrahedron Letters, 2001 , vol. 42, # 5 p. 961 - 964
