6H-苯并[c]苯并吡喃合成路线 （共 63 条）
反应条件
1: potassium carbonate / acetone / Inert atmosphere; Reflux
2: water; palladium diacetate; triphenylphosphine; sodium t-butanolate / 1-methyl-pyrrolidin-2-one / 75 °C / Inert atmosphere
View Scheme
参考文献
Shen, Zengming; Ni, Zhenjie; Mo, Song; Wang, Jing; Zhu, Yamin
Chemistry - A European Journal, 2012 , vol. 18, # 16 p. 4859 - 4865
反应条件
sulfuric acid
T=65°C; 25 h; Reflux;
参考文献
He, Hua-Feng; Wang, Kai; Xing, Bo; Sheng, Guorong; Ma, Tingxuan; Bao, Weiliang
Synlett, 2013 , vol. 24, # 2 art. no. ST-2012-W0886-L, p. 211 - 214
反应条件
in water; acetonitrile
0.666667 h; Irradiation;
参考文献
Huang, C.-G.; Wan, Peter
Journal of Organic Chemistry, 1991 , vol. 56, # 16 p. 4846 - 4853
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 60 °C
2: tetrabutylammomium bromide; potassium acetate; palladium diacetate / N,N-dimethyl acetamide; water / 6 h / 90 °C / Sonication; Inert atmosphere
View Scheme
参考文献
Zhang, Lei; Geng, Mei; Teng, Peng; Zhao, Dan; Lu, Xi; Li, Jian-Xin
Ultrasonics Sonochemistry, 2012 , vol. 19, # 2 p. 250 - 256
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 60 °C
2: tetrabutylammomium bromide; potassium acetate; palladium diacetate / N,N-dimethyl acetamide; water / 6 h / 90 °C / Sonication; Inert atmosphere
View Scheme
参考文献
Zhang, Lei; Geng, Mei; Teng, Peng; Zhao, Dan; Lu, Xi; Li, Jian-Xin
Ultrasonics Sonochemistry, 2012 , vol. 19, # 2 p. 250 - 256
反应条件
1: potassium carbonate / acetonitrile / 12 h / |Inert atmosphere; |Schlenk technique; |Reflux
2: potassium hexamethylsilazane; [(((2,6-CHMe2)2C6H3N=CMe)2C5H3N)FeBr2] / benzene / 18 h / 80 °C / |Inert atmosphere; |Schlenk technique
View Scheme
参考文献
Salanouve, Elise; Bouzemame, Ghania; Blanchard, Sebastien; Derat, Etienne; Desage-El Murr, Marine; Fensterbank, Louis
Chemistry - A European Journal, 2014 , vol. 20, # 16 p. 4754 - 4761
反应条件
in water; acetonitrile
Irradiation; Yield given;
参考文献
Wan, Peter; Huang, Cai-Gu
Journal of the Chemical Society, Chemical Communications, 1988 , # 17 p. 1193 - 1195
参考文献
Inubushi
Yakugaku Zasshi, 1952 , vol. 72, p. 656
Chem.Abstr., 1953 , p. 2173
反应条件
in water; acetonitrile
2 h; Irradiation;
参考文献
Huang, C.-G.; Shukla, Deepak; Wan, Peter
Journal of Organic Chemistry, 1991 , vol. 56, # 18 p. 5437 - 5442
反应条件
1: LiAlH4; diethyl ether
2: benzene; HBr
3: ethanolic KOH-solution
View Scheme
参考文献
Inubushi
Yakugaku Zasshi, 1952 , vol. 72, p. 656
Chem.Abstr., 1953 , p. 2173
