3-三乙基硅烷基丙-1-醇合成路线 (共 9 条)
反应条件
in not given oxidn. of diboryl compd.; detected by GC analysis and (13)C-NMR;
参考文献
Soderquist, John A.; Colberg, Juan C.; Valle, Luis Del
Journal of the American Chemical Society, 1989 , vol. 111, # 13 p. 4873 - 4878
反应条件
1: H2PtCl6 2: TsOH, MeOH View Scheme
参考文献
Sheludyakov,V.D. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1972 , vol. 42, # 10 p. 2209 - 2213,2205 - 2209
反应条件
Yield given. Multistep reaction;
参考文献
Soderquist, John A.; Colberg, Juan C.; Valle, Luis Del
Journal of the American Chemical Society, 1989 , vol. 111, # 13 p. 4873 - 4878
反应条件
methanol; toluene-4-sulfonic acid
参考文献
Sheludyakov,V.D. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1972 , vol. 42, # 10 p. 2209 - 2213,2205 - 2209
反应条件
hydrogenchloride; methanol
参考文献
Grishko,A.N.; Samokhvalov,N.M.
J. Gen. Chem. USSR (Engl. Transl.), 1977 , vol. 47, # 2 p. 377 - 379,349 - 351
反应条件
(i) H2PtCl6*6H2O, iPrOH, (ii) aq. HF; Multistep reaction;
参考文献
Grishko,A.N.; Samokhvalov,N.M.
J. Gen. Chem. USSR (Engl. Transl.), 1977 , vol. 47, # 2 p. 377 - 379,349 - 351
参考文献
Lukevits,E.A.; Voronkov,M.G.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1965 , vol. 1, p. 116 - 121
Khimiya Geterotsiklicheskikh Soedinenii, 1965 , vol. 1, # 2 p. 179 - 186
反应条件
H2PtCl6 fixed on anion exchanger AV-17-8 T=20°C; ΔE(activ.); other temperatures; Thermodynamic dataRate constant;
参考文献
Zaslavskaya, T. N.; Reikhsfel'd, V. O.; Filippov, N. A.; Shornik, N. A.
J. Gen. Chem. USSR (Engl. Transl.), 1980 , vol. 50, # 11 p. 2478 - 2482,2001 - 2005
反应条件
sulfuric acid in benzene
参考文献
Mironov,V.F. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1967 , vol. 37, # 7 p. 1669 - 1673,1588 - 1591