2-脱氧-b-D-吡喃核糖合成路线 (共 27 条)
反应条件
1: methanol With acetyl chloride T=20°C; Inert atmosphere; 2: 2-deoxy-D-arabinopyranose T=20°C; Inert atmosphere;
参考文献
Tetrahedron, , vol. 65, # 41 p. 8461 - 8467
反应条件
hydrogenchloride 15 h; Ambient temperature; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 60, # 16 p. 5170 - 5173
反应条件
1: HCl / 0.42 h / Ambient temperature 2: pyridine / Ambient temperature 3: HCl 4: 15 percent Spectr. / CDCl3 / 1 h View Scheme
参考文献
Rolland, Valerie; Kotera, Mitsuharu; Lhomme, Jean
Synthetic Communications, 1997 , vol. 27, # 20 p. 3505 - 3511
反应条件
diclazuril in water-d2 T=43.3°C; Equilibrium constantRate constant;
参考文献
Bauer, Hans; Brinkmeier, Arno; Buddrus, Joachim; Jablonowski, Maria
Liebigs Annalen der Chemie, 1986 , # 10 p. 1804 - 1808
反应条件
1: HCl / 0.42 h / 20 °C 2: pyridine / 20 °C View Scheme
参考文献
Rolland, Valerie; Kotera, Mitsuharu; Lhomme, Jean
Synthetic Communications, 1997 , vol. 27, # 20 p. 3505 - 3511
反应条件
1: HCl / 0.42 h / Ambient temperature 2: pyridine / Ambient temperature 3: HCl View Scheme
参考文献
Rolland, Valerie; Kotera, Mitsuharu; Lhomme, Jean
Synthetic Communications, 1997 , vol. 27, # 20 p. 3505 - 3511
反应条件
1: methanol With acetyl chloride T=20°C; Inert atmosphere; 2: 2-deoxy-D-arabinopyranose T=20°C; Inert atmosphere;
参考文献
Ludek, Olaf R.; Marquez, Victor E.
Tetrahedron, 2009 , vol. 65, # 41 p. 8461 - 8467
反应条件
hydrogenchloride 15 h; Ambient temperature; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Jandu; Selwood
Journal of Organic Chemistry, 1995 , vol. 60, # 16 p. 5170 - 5173
反应条件
hydrogenchloride T=20°C; 2 h;
参考文献
Ajinomoto Co., Inc.
Patent: EP1574515 A2, 2005 ;
Location in patent: Page/Page column 15-16 ;
反应条件
Acidic conditions; Product distribution / selectivity;
参考文献
Storer, Richard; Moussa, Adel; Wang, Jingyang; Chaudhuri, Narayan C.; Mathieu, Steven; Stewart, Alistair
Patent: US2005/59632 A1, 2005 ;
Location in patent: Page/Page column 19; 20 ;