2-(2-溴苯基)苯并噻唑合成路线 (共 9 条)
反应条件
1,4-diaza-bicyclo[2.2.2]octane; 1,10-phenanthroline; copper (II) acetate monohydrate; sulfur in dimethyl sulfoxide
T=100°C;
参考文献
Wang, Rui; Ding, Yong-Liang; Liu, Hong; Peng, Shu; Ren, Jie; Li, Lei
Tetrahedron Letters, 2014 , vol. 55, # 4 p. 945 - 949
反应条件
iron(III) chloride adsorbed on silica gel; dihydrogen peroxide in ethanol; water
T=20°C; 0.133333 h;
参考文献
Mosslemin, Mohammad Hossein; Fazlinia, Abbas
Phosphorus, Sulfur and Silicon and the Related Elements, 2010 , vol. 185, # 10 p. 2165 - 2170
反应条件
oxygen; copper diacetate in dimethyl sulfoxide
T=130°C; 44 h; Sealed tube;
参考文献
Song, Qiuling; Feng, Qiang; Zhou, Mingxin
Organic Letters, 2013 , vol. 15, # 23 p. 5990 - 5993
反应条件
sodium dithionite in dimethyl sulfoxide
T=80°C; 4 h; Molecular sieve;
参考文献
Wang, Zhanglin; Tang, Riyuan; Xiao, Qin
Chinese Journal of Chemistry, 2011 , vol. 29, # 2 p. 314 - 320
反应条件
[Fe(phthalocyanine)]; sodium t-butanolate in toluene
T=120°C; 36 h; Inert atmosphere;
参考文献
Bala, Manju; Verma, Praveen Kumar; Sharma, Upendra; Kumar, Neeraj; Singh, Bikram
Green Chemistry, 2013 , vol. 15, # 6 p. 1687 - 1693
反应条件
Iron (III) nitrate nonahydrate; oxygen; [(t-Bu)3PH]BF4 in water; dimethyl sulfoxide
T=120°C; 24 h; Sealed tubeGreen chemistry;
参考文献
Khemnar, Ashok B.; Bhanage, Bhalchandra M.
RSC Advances, 2014 , vol. 4, # 18 p. 8939 - 8942
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in tetrahydrofuran; water
Inert atmosphereSchlenk technique;
参考文献
Rao, Ying-Li; Amarne, Hazem; Chen, Leanne D.; Brown, Matthew L.; Mosey, Nicholas J.; Wang, Suning
Journal of the American Chemical Society, 2013 , vol. 135, # 9 p. 3407 - 3410
反应条件
1: N,N-dimethyl-formamide / 140 °C / |Microwave irradiation
2: N,N-dimethyl-formamide / 140 °C / |Microwave irradiation
3: N,N-dimethyl-formamide / 140 °C / |Microwave irradiation
View Scheme
参考文献
Lin, Yu-Chin; Li, Ni-Ching; Cherng, Yie-Jia
Journal of Heterocyclic Chemistry, 2014 , vol. 51, # 3 p. 808 - 814
反应条件
1: N,N-dimethyl-formamide / 140 °C / |Microwave irradiation
2: N,N-dimethyl-formamide / 140 °C / |Microwave irradiation
3: N,N-dimethyl-formamide / 140 °C / |Microwave irradiation
View Scheme
参考文献
Lin, Yu-Chin; Li, Ni-Ching; Cherng, Yie-Jia
Journal of Heterocyclic Chemistry, 2014 , vol. 51, # 3 p. 808 - 814