1-氧杂螺[2.3]己-2-基甲醇合成路线 (共 3 条)
反应条件
peracetic acid; sodium carbonate in 1,2-dichloro-ethane Epoxidation; 7.25 h; Heating;
参考文献
Afzal, Mohammad; Walton, John C.
Journal of the Chemical Society. Perkin Transactions 2, 1999 , # 5 p. 937 - 945
反应条件
1: 36 percent / DIBAL-H / tetrahydrofuran 2: 86 percent / sodium carbonate; peroxyacetic acid / 1,2-dichloro-ethane / 7.25 h / Heating View Scheme
参考文献
Afzal, Mohammad; Walton, John C.
Journal of the Chemical Society. Perkin Transactions 2, 1999 , # 5 p. 937 - 945
反应条件
1: triethylamine / CH2Cl2 2: 1.09 g / lithium bromide / acetone / Heating 3: 22 percent Spectr. / triphenyltin hydride / benzene-d6 / 4 h / 80 °C View Scheme
参考文献
Afzal, Mohammad; Walton, John C.
Journal of the Chemical Society. Perkin Transactions 2, 1999 , # 5 p. 937 - 945