sulfur(IV) fluoride 24 h; Ambient temperature;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '11342940', constants.ctx, '0')">sodium hydroxide</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1098229', constants.ctx, '0')">methanol</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '3587155', constants.ctx, '0')">water</a> <br />1&nbsp;h;&nbsp;&nbsp;Heating;&nbsp;<br /> &nbsp;

<b>Multi-step reaction with 11 steps<br /> </b>1: methanol<br />2: H₂O/KOH / ethanol / 16 h / Ambient temperature<br />3: hydrazine hydrate, KOH / bis-(2-hydroxy-ethyl) ether / 10 h / Heating<br />4: 91 percent / concn H₂SO₄ / 1,2-dichloro-ethane / 20 h / Heating<br />5: 92 percent / BF₃*OEt₂ / Ambient temperature<br />6: 94 percent / NaOMe / methanol / 2 h / Heating<br />7: 92 percent / SF₄ / 24 h / Ambient temperature<br />8: 96 percent / H₂O/KOH / ethanol / 16 h / Ambient temperature<br />9: 90 percent / diethyl ether; hexane / 2 h / Heating<br />10: 77 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 72 h / Ambient temperature<br />11: 93 percent / NaOMe / methanol / 2 h / Heating<br /> <br /> &nbsp;

<b>Multi-step reaction with 10 steps<br /> </b>1: H₂O/KOH / ethanol / 16 h / Ambient temperature<br />2: hydrazine hydrate, KOH / bis-(2-hydroxy-ethyl) ether / 10 h / Heating<br />3: 91 percent / concn H₂SO₄ / 1,2-dichloro-ethane / 20 h / Heating<br />4: 92 percent / BF₃*OEt₂ / Ambient temperature<br />5: 94 percent / NaOMe / methanol / 2 h / Heating<br />6: 92 percent / SF₄ / 24 h / Ambient temperature<br />7: 96 percent / H₂O/KOH / ethanol / 16 h / Ambient temperature<br />8: 90 percent / diethyl ether; hexane / 2 h / Heating<br />9: 77 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 72 h / Ambient temperature<br />10: 93 percent / NaOMe / methanol / 2 h / Heating<br /> <br /> &nbsp;