1,1-二甲基硅杂环丁烷 二甲基三亚甲基硅烷合成路线 （共 97 条）
反应条件
magnesium; ethylene dibromide in dibutyl diglyme T=20 - 95°C; Grignard Reaction; 2 h;
参考文献
WO2008/33980 A2, ;
Page/Page column 7 ;
反应条件
magnesium in diethyl ether 48 h;
参考文献
Journal of Organometallic Chemistry, , vol. 188, # 1 p. 25 - 52
反应条件
in diethyl ether T=-78 - 20°C;
参考文献
Journal of Organometallic Chemistry, , vol. 188, # 1 p. 25 - 52
反应条件
in diethyl ether T=37°C; 3 h;
参考文献
Journal of Organometallic Chemistry, , vol. 188, # 1 p. 25 - 52
反应条件
in diethyl ether T=-78 - 20°C;
参考文献
Journal of Organometallic Chemistry, , vol. 188, # 1 p. 25 - 52
反应条件
in diethyl ether T=20°C; 3 h;
参考文献
Journal of Organometallic Chemistry, , vol. 188, # 1 p. 25 - 52
反应条件
potassium-sodium in gaseous matrix T=280 - 320°C; P=0.1 - 1 Torr; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organometallic Chemistry, , vol. 292, p. 189 - 204
反应条件
sulfuric acid; ammonium chloride anschliessend Behandeln mit Magnesium in Aether;
参考文献
Journal of the American Chemical Society, , vol. 76, p. 5002
反应条件
T=500°C; P=1 Torr; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 45, # 3 p. 541 - 543
反应条件
tert.-butyl lithium in pentane T=-20°C;
参考文献
Journal of Organometallic Chemistry, , vol. 336, p. 83 - 104
