1,3-二乙基四甲基二硅烷合成路线 （共 17 条）
反应条件
ethanol; hydrogen fluoride
参考文献
Eaborn, C.
Journal of the Chemical Society, 1952 , p. 2846 - 2849
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Eaborn, C.
Journal of the Chemical Society, 1953 , p. 494 - 501
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Gmelin Handbook: Si: MVol.C, 38, page 117 - 119
反应条件
in sulfuric acid aq. H2SO4; ((C2H5)(CH3)2Si)2O and NH4F in concd. H2SO4;;
参考文献
Eaborn, C.
Journal of the Chemical Society, 1949 , p. 2755 - 2764
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Gmelin Handbook: Si: MVol.C, 38, page 117 - 119
反应条件
sulfuric acid; ammonium chloride; sodium chloride
参考文献
Westermark
Acta Chemica Scandinavica (1947-1973), 1955 , vol. 9, p. 947,953
反应条件
hydrogen; (o-OC6H4CH3)3PRuCl(PPh3)2
T=120°C; P=2327.2 Torr; 3 h;
参考文献
Lewis,L.N.
Journal of the American Chemical Society, 1986 , vol. 108, p. 743
反应条件
[(POCOP)Ir(H)(acetone)]+[B(C6F5)4]- in C6D5Cl
T=23°C; P=760.051 Torr; 1.7 h;
参考文献
Park, Sehoon; Bezier, David; Brookhart, Maurice
Journal of the American Chemical Society, 2012 , vol. 134, # 28 p. 11404 - 11407
反应条件
dihydrogen peroxide; methyltrioxorhenium (VII); urea in dichloromethane
T=20°C; 18 h; other trioranosilanes, other reagents, other solvent, var. time; Product distribution;
参考文献
Adam, Waldemar; Mitchell, Catherine M.; Sana-Moeller, Chantu R.; Weichold, Oliver
Journal of the American Chemical Society, 1999 , vol. 121, # 10 p. 2097 - 2103
反应条件
[(POCOP)Ir(H)(acetone)]+[B(C6F5)4]- in C6D4Cl2
T=23°C; 0.3 h;
参考文献
Park, Sehoon; Bezier, David; Brookhart, Maurice
Journal of the American Chemical Society, 2012 , vol. 134, # 28 p. 11404 - 11407
反应条件
carbon monoxide; dicobalt octacarbonyl
参考文献
Seki,Y. et al.
Journal of Organometallic Chemistry, 1977 , vol. 140, p. 361 - 378
反应条件
potassium fluoride in dimethyl sulfoxide
参考文献
Voronkov,M.G. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1975 , vol. 24, p. 1932 - 1934
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1975 , vol. 24, p. 2052 - 2054
反应条件
in not given
hydrolysis;;
参考文献
Dow Corning Corp.
Patent: US2495362 , 1950 ;
C. A., 1950 , p. 5644
