2-(吡啶-4-基)苯并[d]噻唑合成路线 （共 26 条）
反应条件
1-propanephosphonic acid cyclic anhydride; N-ethyl-N,N-diisopropylamine in ethyl acetate
T=100°C; 0.166667 h; Microwave irradiationSealed tube;
参考文献
Wen, Xiaoan; Bakali, Jamal El; Deprez-Poulain, Rebecca; Deprez, Benoit
Tetrahedron Letters, 2012 , vol. 53, # 19 p. 2440 - 2443
参考文献
Kundus, Nabanita; Audhya, Anandalok; Abtab, Sk Md Towsif; Ghosh, Sanjib; Tiekink, Edward R. T.; Chaudhury, Muktimoy
Crystal Growth and Design, 2010 , vol. 10, # 3 p. 1269 - 1282
反应条件
boron trifluoride diethyl etherate in 1,4-dioxane
T=20 - 100°C; Inert atmosphere;
参考文献
Bommegowda, Yadaganahalli K.; Lingaraju, Gejjalagere S.; Thamas, Saji; Vinay Kumar, Koravangala S.; Pradeepa Kumara, Challanayakanahally S.; Rangappa, Kanchugarakoppal S.; Sadashiva, Marilinganadoddi P.
Tetrahedron Letters, 2013 , vol. 54, # 21 p. 2693 - 2695
反应条件
palladium diacetate
T=60 - 75°C; 10 h; Ionic liquid;
参考文献
Kalkhambkar, Rajesh G.; Laali, Kenneth K.
Tetrahedron Letters, 2012 , vol. 53, # 32 p. 4212 - 4215
反应条件
1,4-diaza-bicyclo[2.2.2]octane; 1,10-phenanthroline; copper (II) acetate monohydrate; sulfur in dimethyl sulfoxide
T=100°C;
参考文献
Wang, Rui; Ding, Yong-Liang; Liu, Hong; Peng, Shu; Ren, Jie; Li, Lei
Tetrahedron Letters, 2014 , vol. 55, # 4 p. 945 - 949
反应条件
oxygen in dimethyl sulfoxide; chlorobenzene
T=140°C; P=760.051 Torr; 16 h; Sealed tube;
参考文献
Liao, Yunfeng; Qi, Hongrui; Chen, Shanping; Jiang, Pengcheng; Zhou, Wang; Deng, Guo-Jun
Organic Letters, 2012 , vol. 14, # 23 p. 6004 - 6007
反应条件
iodine in acetonitrile
T=20°C; 0.5 h;
参考文献
Naresh, Gunaganti; Kant, Ruchir; Narender, Tadigoppula
Journal of Organic Chemistry, 2014 , vol. 79, # 9 p. 3821 - 3829
反应条件
sulfur in neat (no solvent)
T=120°C; 24 h; Sealed tubeInert atmosphere; ConcentrationTemperature;
参考文献
Nguyen, Thanh Binh; Ermolenko, Ludmila; Al-Mourabit, Ali
Organic Letters, 2013 , vol. 15, # 16 p. 4218 - 4221
反应条件
1: 2-amino-benzenethiol With trimethylaluminum chloride in toluene
T=0 - 20°C;
2: hydroxymethyl JandaJelTM resin-bound 4-pyridyl ester in toluene
24 h; Heating; Further stages.;
参考文献
Matsushita, Hana; Lee, Sang-Hyeup; Joung, Meyoungju; Clapham, Bruce; Janda, Kim D.
Tetrahedron Letters, 2004 , vol. 45, # 2 p. 313 - 316
反应条件
PdCl(C3H5)(1,4-bis(diphenylphosphino)butane); caesium carbonate in N,N-dimethyl-formamide
T=150°C; 20 h; Inert atmosphere;
参考文献
Derridj, Fazia; Roger, Julien; Geneste, Florence; Djebbar, Safia; Doucet, Henri
Journal of Organometallic Chemistry, 2009 , vol. 694, # 3 p. 455 - 465
