[4-(氯磺酰基)苯基]乙酸合成路线 （共 7 条）
反应条件
chlorosulfonic acid T=0 - 20°C; 13 h;
参考文献
Kim, Kyung Ju; Choi, Min Ji; Shin, Ji-Sun; Kim, Minju; Choi, Hye-Eun; Kang, Seoung Mook; Jin, Jae Ho; Lee, Kyung-Tae; Lee, Jae Yeol
Bioorganic and Medicinal Chemistry Letters, 2014 , vol. 24, # 8 p. 1958 - 1962
反应条件
chlorosulfonic acid T=0 - 20°C; Neat (no solvent);
参考文献
Starnes JR., William Herbert; Du, Bin
Patent: US2005/49307 A1, 2005 ;
Location in patent: Page/Page column 13 ;
参考文献
EUROSCREEN S.A.
Patent: WO2009/10478 A2, 2009 ;
Location in patent: Page/Page column 91 ;
WO 2009/010478 A2
反应条件
1: With phosphorus; iodine in acetic acid T=100 - 110°C; 0.5 - 4 h; Heating / reflux; 2: With water T=100°C; 1.5 - 2 h; Heating / reflux; Product distribution / selectivity;
参考文献
Starnes JR., William Herbert; Du, Bin
Patent: US2005/49307 A1, 2005 ;
Location in patent: Page/Page column 14 ;
反应条件
4-MeC6H4SNa in ethanol
参考文献
Tetrahedron Letters, , vol. 26, # 32 p. 3879 - 3882
反应条件
1: With phosphorus; iodine in acetic acid T=100 - 110°C; 0.5 - 4 h; Heating / reflux; 2: With water T=100°C; 1.5 - 2 h; Heating / reflux; Product distribution / selectivity;
参考文献
Starnes JR., William Herbert; Du, Bin
Patent: US2005/49307 A1, 2005 ;
Location in patent: Page/Page column 14 ;
反应条件
potassium fluoride; 18-crown-6 ether in acetonitrile
4 h;
参考文献
EUROSCREEN S.A.
Patent: WO2009/10478 A2, 2009 ;
Location in patent: Page/Page column 92 ;
WO 2009/010478 A2
