反应条件
1: 97 percent / TEA / CH2Cl2 / 2 h / 0 - 20 °C 2: 38 percent / Oxone; Na2EDTA; Bu4NHSO4 / acetone; aq. phosphate buffer / 5 h / pH 7 3: 100 percent / DBU / CH2Cl2 / 16 h 4: H2 / {[(S,S)-MeDuPHOS]Rh(COD)}BF4 / methanol / 14 h View Scheme
参考文献
Smith, Mark E.B.; Lloyd, Michael C.; Derrien, Nadine; Lloyd, Richard C.; Taylor, Stephen J.C.; Chaplin, David A.; Casy, Guy; McCague, Raymond
Tetrahedron Asymmetry, 2001 , vol. 12, # 5 p. 703 - 705