甲基-(2-对甲苯-乙基)胺合成路线 （共 10 条）
反应条件
hydrogenchloride; water in methanol T=0 - 20°C;
参考文献
Kisic, Andrea; Stephan, Michel; Mohar, Barbara
Organic Letters, 2013 , vol. 15, # 7 p. 1614 - 1617
反应条件
1.1: triethylamine / tetrahydrofuran / 0 - 20 °C 1.2: 1 h 2.1: sodium hydride / tetrahydrofuran / 0.33 h / 0 - 20 °C 2.2: 5 h / 0 - 20 °C 3.1: water; hydrogenchloride / methanol / 0 - 20 °C View Scheme
参考文献
Organic Letters, , vol. 15, # 7 p. 1614 - 1617
反应条件
1.1: sodium hydride / tetrahydrofuran / 0.33 h / 0 - 20 °C 1.2: 5 h / 0 - 20 °C 2.1: water; hydrogenchloride / methanol / 0 - 20 °C View Scheme
参考文献
Organic Letters, , vol. 15, # 7 p. 1614 - 1617
反应条件
borane-THF in tetrahydrofuran 4 h; Inert atmosphereReflux;
参考文献
Journal of the American Chemical Society, , vol. 135, # 19 p. 7304 - 7311
反应条件
1: toluene; water / 0.5 h / 0 - 22 °C / |Inert atmosphere 2: borane-THF / tetrahydrofuran / 4 h / |Inert atmosphere; |Reflux View Scheme
参考文献
Journal of the American Chemical Society, , vol. 135, # 19 p. 7304 - 7311
反应条件
1: N,N-dimethyl-formamide; thionyl chloride / toluene / 0.5 h / 40 °C / |Inert atmosphere 2: toluene; water / 0.5 h / 0 - 22 °C / |Inert atmosphere 3: borane-THF / tetrahydrofuran / 4 h / |Inert atmosphere; |Reflux View Scheme
参考文献
Journal of the American Chemical Society, , vol. 135, # 19 p. 7304 - 7311
反应条件
1: benzene; PBr3 / 0 °C 2: ethanol View Scheme
参考文献
Journal of Organic Chemistry, , vol. 2, p. 139,143
反应条件
1: diethyl ether; benzene / anfangs unter Kuehlung, zuletzt bei Siedetemperatur 2: benzene; PBr3 / 0 °C 3: ethanol View Scheme
参考文献
Journal of Organic Chemistry, , vol. 2, p. 139,143
反应条件
1: diethyl ether / anfangs unter Kuehlung, zuletzt bei Siedetemperatur 2: benzene; PBr3 / 0 °C 3: ethanol View Scheme
参考文献
Journal of Organic Chemistry, , vol. 2, p. 139,143
参考文献
Journal of Organic Chemistry, , vol. 2, p. 139,143
