(2E)-1-(4-氯苯基)-3-苯基-2-丙烯-1-酮合成路线 (共 18 条)
反应条件
potassium carbonate in ethanol Michael addition; 0.233333 h; Heating;
参考文献
Safaei-Ghomi; Bamoniri; Soltanian-Telkabadi
Chemistry of Heterocyclic Compounds, 2006 , vol. 42, # 7 p. 892 - 896
反应条件
dicyclohexyl(2,4,6-triisopropylphenyl)phosphine; potassium carbonate; bis(dibenzylideneacetone)-palladium(0) in isopropyl alcohol T=80°C; 7 h;
参考文献
Bei, Xiaohong; Hagemeyer, Alfred; Volpe, Anthony; Saxton, Robert; Turner, Howard; Guram, Anil S.
Journal of Organic Chemistry, 2004 , vol. 69, # 25 p. 8626 - 8633
反应条件
1: sulfuric acid / methanol / 0.17 h / 50 - 60 °C 2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 2 h / 20 °C View Scheme
参考文献
Desai, Vidya G.; Satardekar, Pooja C.; Polo, Sampada; Dhumaskar, Kashinath
Synthetic Communications, 2012 , vol. 42, # 6 p. 836 - 842
反应条件
hydrogen; palladium in methanol 20 h;
参考文献
Kitamura, Yoshiaki; Tanaka, Asami; Sato, Mutsumi; Oono, Keiji; Ikawa, Takashi; Maegawa, Tomohiro; Monguchi, Yasunari; Sajiki, Hironao
Synthetic Communications, 2007 , vol. 37, # 24 p. 4381 - 4388
反应条件
trifluoroacetic acid 72 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 72, # 24 p. 9383 - 9386
反应条件
in anhydrous butyl ether 12 h; Heating;
参考文献
Guziec, Frank S.; Luzzio, Frederick A.
Journal of Organic Chemistry, 1983 , vol. 48, # 14 p. 2434 - 2437
反应条件
1: NH2OH*HCl; TEA
2: MnO2 / CHCl3 / Heating
View Scheme
参考文献
Kurangi, Reshma F.; Kawthankar, Rima; Sawal, Sulfala; Desai, Vidya G.; Tilve, Santosh G.
Synthetic Communications, 2007 , vol. 37, # 4 p. 587 - 589
反应条件
1: With sodium ethanolate in diethyl ether; ethanol
20 h;
2: With sodium hydroxide in water
6 h; Heating;
参考文献
Sridharan; Muthusubramanian; Sivasubramanian
Journal of Heterocyclic Chemistry, 2005 , vol. 42, # 7 p. 1321 - 1330
反应条件
anhydrous magnesium perchlorate in 1,2-dichloro-ethane
0.5 h; Heating;
参考文献
Khatik, Gopal L.; Kumar, Raj; Chakraborti, Asit K.
Synthesis, 2007 , # 4 p. 541 - 546
反应条件
Bi(NO3)3 on neutral alumina
T=130°C; 4.5 h; Further byproducts given;
参考文献
Verma, Anil K.; Koul, Summon; Razdan, Tej K.; Kapoor, Kamal K.
Canadian Journal of Chemistry, 2006 , vol. 84, # 8 p. 1064 - 1073