反式-薄荷基-2,8-二烯-1-醇合成路线 （共 19 条）
反应条件
Na6(NH4)4lt;(Mn(II)(H2O)3)2(WO2)2(BiW9O33)2gt;*37H2O; dihydrogen peroxide in dichloromethane 8 h; Ambient temperatureother catalysts; var. reaction times; regioselective epoxidation; Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 120, # 29 p. 7252 - 7259
参考文献
Helvetica Chimica Acta, , vol. 63, # 1 p. 76 - 94
反应条件
1: 5-(1-pentyl)resorcinol With toluene-4-sulfonic acid in benzene 2.5 h; 2: (1S,4R)-p-mentha-2,8-dien-1-ol in benzene T=20°C; 0.5 h;
参考文献
AllTranz Inc.
Patent: US2009/36523 A1, 2009 ;
Location in patent: Page/Page column 12 ;
反应条件
aluminum oxide; boron trifluoride diethyl etherate in dichloromethane T=40 - 41°C; 0.00277778 h;
参考文献
Tetrahedron Letters, , vol. 26, # 8 p. 1083 - 1086
反应条件
aluminum oxide; boron trifluoride diethyl etherate in dichloromethane T=40 - 41°C; 0.00277778 h;
参考文献
Baek, Seung-Hwa; Srebnik, Morris; Mechoulam, Raphael
Tetrahedron Letters, 1985 , vol. 26, # 8 p. 1083 - 1086
反应条件
1.1: TsOH / benzene / Heating 2.1: NaH / tetrahydrofuran / 0 °C 2.2: tetrahydrofuran 3.1: Li; NH3 / tetrahydrofuran; diethyl ether / -78 °C View Scheme
参考文献
Huffman, John W.; Liddle, John; Yu, Shu; Aung, Mie Mie; Abood, Mary E.; Wiley, Jenny L.; Martin, Billy R.
Bioorganic and Medicinal Chemistry, 1999 , vol. 7, # 12 p. 2905 - 2914
反应条件
toluene-4-sulfonic acid in dichloromethane 2.75 h; Heating;
参考文献
Crombie, Leslie; Crombie, W. Mary L.; Tuchinda, Patoomratana
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 1255 - 1262
反应条件
aluminum oxide; boron trifluoride diethyl etherate in dichloromethane
T=40 - 41°C; 0.00277778 h;
参考文献
Baek, Seung-Hwa; Srebnik, Morris; Mechoulam, Raphael
Tetrahedron Letters, 1985 , vol. 26, # 8 p. 1083 - 1086
参考文献
Petrzilka,T. et al.
Helvetica Chimica Acta, 1969 , vol. 52, # 4 p. 1102 - 1134
