1-(1-乙基丙基)-4-甲苯合成路线 (共 10 条)
反应条件
tris(2,4-di-tert-butyl-phenyl) phosphite; iron(III) chloride in diethyl ether
0.5 h; Heating;
参考文献
Bedford, Robin B.; Betham, Michael; Bruce, Duncan W.; Danopoulos, Andreas A.; Frost, Robert M.; Hird, Michael
Journal of Organic Chemistry, 2006 , vol. 71, # 3 p. 1104 - 1110
反应条件
silica-supported aluminum chloride in dichloromethane
T=140°C; Friedel-Crafts Alkylation; 0.0833333 h; Microwave irradiation; Overall yield = 65 percent;
参考文献
Zupp, Laurine R.; Campanella, Veronica L.; Rudzinski, Diandra M.; Beland, Franois; Priefer, Ronny
Tetrahedron Letters, 2012 , vol. 53, # 39 p. 5343 - 5346
反应条件
anthracene; sodium
T=225°C; P=22065.2 Torr;
参考文献
Pines et al.
Journal of the American Chemical Society, 1955 , vol. 77, p. 554,555
反应条件
Cl2Ni(1,2-bis(diphenylphosphino)ethane) in diethyl ether; benzene
16 h; Heating;
参考文献
Tzeng, Yih-Ling; Yang, Ping-Fan; Mei, Nai-Wen; Yuan, Tien-Min; Yu, Chun-Chi; Luh, Tien-Yau
Journal of Organic Chemistry, 1991 , vol. 56, # 18 p. 5289 - 5293
反应条件
sulfuric acid; boron trifluoride
参考文献
Hennion; Kurtz
Journal of the American Chemical Society, 1943 , vol. 65, p. 1001
反应条件
Erhitzen des erhaltenen 3-p-Tolyl-pentan-3-ols mit Oxalsaeure und Hydrieren des Reaktionsprodukts an Kupferoxid-Chromoxid bei 75grad/100 at;
参考文献
Pines et al.
Journal of the American Chemical Society, 1955 , vol. 77, p. 554,555
反应条件
T=200 - 225°C; P=22065.2 Torr;
参考文献
Pines et al.
Journal of the American Chemical Society, 1955 , vol. 77, p. 554,555
反应条件
montmorillonite doped with TiCl4
6 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Laszlo, Pierre; Mathy, Arthur
Helvetica Chimica Acta, 1987 , vol. 70, p. 577 - 586
反应条件
(i) Mg, Et2O, (ii) I2, (iii) H2; Multistep reaction;
参考文献
Kovacic,P. et al.
Journal of Organic Chemistry, 1968 , vol. 33, p. 4515 - 4520
反应条件
montmorillonite doped with TiCl4
6 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Laszlo, Pierre; Mathy, Arthur
Helvetica Chimica Acta, 1987 , vol. 70, p. 577 - 586