3,3',5,5'-四甲氧基-联苄基合成路线 （共 27 条）
反应条件
iodine; magnesium in diethyl ether 2.5 h; Heating;
参考文献
Crombie, Leslie; Jamieson, Sally V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 1467 - 1476
反应条件
manganese in tetrahydrofuran T=20°C; 0.166667 h;
参考文献
Suh, YoungSung; Lee, Jun-Sik; Kim, Seoung-Hoi; Rieke, Reuben D.
Journal of Organometallic Chemistry, 2003 , vol. 684, # 1-2 p. 20 - 36
反应条件
1: With sodium in tetrahydrofuran T=20°C; 18 h; 2: With water in tetrahydrofuran T=0°C;
参考文献
Azzena, Ugo; Dettori, Giovanna; Idini, Maria Vittoria; Pisano, Luisa; Sechi, Grazia
Tetrahedron, 2003 , vol. 59, # 40 p. 7961 - 7966
反应条件
1: With 2,2,6,6-tetramethyl-piperidine; n-butyllithium; potassium tert-butylate in tetrahydrofuran T=-78°C; 0.25 h; Inert atmosphere; 2: With ethylene dibromide in tetrahydrofuran T=-78 - 20°C; Inert atmosphere; regioselective reaction;
参考文献
Blangetti, Marco; Fleming, Patricia; O'Shea, Donal F.
Journal of Organic Chemistry, 2012 , vol. 77, # 6 p. 2870 - 2877
反应条件
ammonia; lithium in tetrahydrofuran 1 h;
参考文献
Saa, Jose M.; Dopico, Mercedes; Martorell, Gabriel; Garcia-Raso, Angel
Journal of Organic Chemistry, 1990 , vol. 55, # 3 p. 991 - 995
反应条件
hydrogen; palladium on activated charcoal in ethanol Yield given;
参考文献
Jo, Geunhyeong; Hyun, Jiye; Hwang, Doseok; Lee, Young Han; Koh, Dongsoo; Lim, Yoongho
Magnetic Resonance in Chemistry, 2011 , vol. 49, # 6 p. 374 - 377
反应条件
1: pyridine / benzene / Ambient temperature 2: 2 percent Chromat. / Irradiation View Scheme
参考文献
Petrzilka,T. et al.
Helvetica Chimica Acta, 1969 , vol. 52, # 4 p. 1102 - 1134
反应条件
1: 1 M B2H6 / tetrahydrofuran 2: pyridine / benzene / Ambient temperature 3: 2 percent Chromat. / Irradiation View Scheme
参考文献
Petrzilka,T. et al.
Helvetica Chimica Acta, 1969 , vol. 52, # 4 p. 1102 - 1134
反应条件
1: 36 percent / potassium tert-butoxide / benzene / 1.) room temp., 20 h, 2.) 60 deg C, 1 h 2: H2 / 10percent Pd/C / ethanol View Scheme
参考文献
Eiden; Gerstlauer
Archiv der Pharmazie, 1981 , vol. 314, # 12 p. 995 - 1006
反应条件
1: 36 percent / potassium tert-butoxide / benzene / 1.) room temp., 20 h, 2.) 60 deg C, 1 h 2: H2 / 10percent Pd/C / ethanol View Scheme
参考文献
Eiden; Gerstlauer
Archiv der Pharmazie, 1981 , vol. 314, # 12 p. 995 - 1006
