2,5-二乙基-1,3-噁唑-4-羧酸乙酯合成路线 (共 17 条)
反应条件
thionyl chloride; benzene
参考文献
Chemische Berichte, , vol. 84, p. 96,99
反应条件
potassium hydroxide in ethanol T=0°C; 0.0833333 h;
参考文献
Sano, Shigeki; Shimizu, Hisashi; Kim, Kweon; Lee, Woo Song; Shiro, Motoo; Nagao, Yoshimitsu
Chemical and Pharmaceutical Bulletin, 2006 , vol. 54, # 2 p. 196 - 203
反应条件
1: CH3COOH; H2 / Pd/C / 1.5 h / 2585.74 Torr 2: SOCl2 / benzene / 1.5 h / 23 - 30 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 128, # 16 p. 5310 - 5311
反应条件
T=540 - 600°C; P=0.01 Torr; 1 h;
参考文献
Ang, Kiah H.; Prager, Rolf H.; Smith, Jason A.; Weber, Ben; Williams, Craig M.
Tetrahedron Letters, 1996 , vol. 37, # 5 p. 675 - 678
反应条件
1,10-phenanthroline; tris(acetonitrile)(η5-2,4-cyclopentadien-1-yl)ruthenium(1+) hexafluorophosphate(1-) T=60°C; 1 h; Inert atmosphere;
参考文献
Austeri, Martina; Rix, Diane; Zeghida, Walid; Lacour, Jerome
Organic Letters, 2011 , vol. 13, # 6 p. 1394 - 1397
反应条件
hydrogenchloride; rhenium heptasulfide T=80°C; 2 h;
参考文献
Chemische Berichte, , vol. 117, # 4 p. 1497 - 1512
反应条件
1: 84 percent / NaN3 / H2O; acetic acid / 40 h / 40 °C 2: 35 percent / 2.2 M HCl / 1 mol-percent Re2S7 / 2 h / 80 °C View Scheme
参考文献
Chemische Berichte, , vol. 117, # 4 p. 1497 - 1512
反应条件
triethylamine in benzene 2.5 h; Heating;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 50, # 7 p. 1788 - 1792
反应条件
1: NBS 2: Et3N / benzene / 2.5 h / Heating View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 50, # 7 p. 1788 - 1792
反应条件
phosphorus pentoxide in chloroform (heating);
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 32, p. 2348 - 2353,2315 - 2320