1-(2,4-二甲基-5-恶唑基)-乙酮合成路线 (共 6 条)
反应条件
[bis(acetoxy)iodo]benzene; boron trifluoride diethyl etherate in 1,2-dichloro-ethane 0.5 h; Reflux;
参考文献
Zheng, Yunhui; Li, Xuming; Ren, Chengfeng; Zhang-Negrerie, Daisy; Du, Yunfei; Zhao, Kang
Journal of Organic Chemistry, 2012 , vol. 77, # 22 p. 10353 - 10361
反应条件
1: acetylacetone With PhI(ODNs)OH 0.0111111 h; microwave irradiation; 2: acetamide 0.0333333 h; microwave irradiation;
参考文献
Lee, Jong Chan; Choi, Hyun Jung; Lee, Yong Chan
Tetrahedron Letters, 2003 , vol. 44, # 1 p. 123 - 125
参考文献
Jaworski, Tadeusz; Mizerski, Tadeusz
Polish Journal of Chemistry, 1981 , vol. 55, # 1 p. 47 - 56
反应条件
in acetic acid 4 h; Heating;
参考文献
Valgimigli, Luca; Brigati, Giovanni; Pedulli, Gian Franco; DiLabio, Gino A.; Mastragostino, Marina; Arbizzani, Catia; Pratt, Derek A.
Chemistry - A European Journal, 2003 , vol. 9, # 20 p. 4997 - 5010
反应条件
T=190°C; 15 h; Yield given. Yields of byproduct given;
参考文献
Jaworski, Tadeusz; Mizerski, Tadeusz
Polish Journal of Chemistry, 1981 , vol. 55, # 1 p. 47 - 56
反应条件
ammonium hydroxide
T=180°C; 10 h;
参考文献
Valgimigli, Luca; Brigati, Giovanni; Pedulli, Gian Franco; DiLabio, Gino A.; Mastragostino, Marina; Arbizzani, Catia; Pratt, Derek A.
Chemistry - A European Journal, 2003 , vol. 9, # 20 p. 4997 - 5010