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乙二醇
甲醛
63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
23018-39-5
合成路线
(共 9 条)
81064-10-0
→
反应条件
23018-39-5
+
81064-14-4
反应条件
Sodium 2,4,6-trimethylbenzenethiolate in dimethyl sulfoxide T=120°C; 0.666667 h;
参考文献
Novi, Marino; Dell'Erba, Carlo; Garbarino, Giacomo; Sancassan, Fernando
Journal of Organic Chemistry, 1982 , vol. 47, # 12 p. 2292 - 2298
6127-91-9
+
81064-10-0
→
反应条件
23018-39-5
+
81064-14-4
反应条件
in dimethyl sulfoxide T=120°C; 0.666667 h;
参考文献
Novi, Marino; Dell'Erba, Carlo; Garbarino, Giacomo; Sancassan, Fernando
Journal of Organic Chemistry, 1982 , vol. 47, # 12 p. 2292 - 2298
81064-10-0
→
反应条件
反应条件
in dimethyl sulfoxide T=20°C; controlled-potential electrolyses;
参考文献
Novi, Marino; Dell'Erba, Carlo; Garbarino, Giacomo; Scarponi, Giuseppe; Capodaglio, Gabriele
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1984 , # 5 p. 951 - 954
81064-10-0
→
反应条件
反应条件
tetra-n-butylammonium acetate in dimethyl sulfoxide controlled-potential electrolysis; 0.1M tetrabutylammonium tetrafluoroborate, platinum bead electrode; Yield given. Yields of byproduct given;
参考文献
Novi, Marino; Garbarino, Giacomo; Petrillo, Giovanni; Dell'Erba, Carlo
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1987 , p. 623 - 632
81064-10-0
+
108-98-5
硫酚
→
反应条件
反应条件
benzenethiol sodium salt in dimethyl sulfoxide T=50°C; 0.166667 h; Irradiationvarious ratios of educts; Product distributionRate constantMechanism;
参考文献
Novi, Marino; Garbarino, Giacomo; Dell'Erba, Carlo
Journal of Organic Chemistry, 1984 , vol. 49, # 15 p. 2799 - 2803
930-69-8
苯硫酚钠
+
81064-10-0
→
反应条件
反应条件
tetra-n-butylammonium tetrafluoroborate in dimethyl sulfoxide electrolysis;
参考文献
Novi, Marino; Garbarino, Giacomo; Dell'Erba, Carlo; Petrillo, Giovanni
Journal of the Chemical Society, Chemical Communications, 1984 , # 18 p. 1205 - 1207
81064-10-0
→
反应条件
23018-39-5
反应条件
in dimethyl sulfoxide controlled-potential electrolysis; 0.1M tetrabutylammonium tetrafluoroborate, platinum bead electrode; Yield given. Yields of byproduct given;
参考文献
Novi, Marino; Garbarino, Giacomo; Petrillo, Giovanni; Dell'Erba, Carlo
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1987 , p. 623 - 632
81064-10-0
+
110348-49-7
→
反应条件
反应条件
in dimethyl sulfoxide controlled-potential electrolysis; 0.1M tetrabutylammonium tetrafluoroborate, platinum bead electrode; Yield given. Yields of byproduct given;
参考文献
Novi, Marino; Garbarino, Giacomo; Petrillo, Giovanni; Dell'Erba, Carlo
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1987 , p. 623 - 632
4670-62-6
苯硫酚四丁基铵
+
81064-10-0
→
反应条件
反应条件
in dimethyl sulfoxide controlled-potential electrolysis; 0.1M tetrabutylammonium tetrafluoroborate, platinum bead electrode; Yield given. Yields of byproduct given;
参考文献
Novi, Marino; Garbarino, Giacomo; Petrillo, Giovanni; Dell'Erba, Carlo
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1987 , p. 623 - 632