tert.-butyl lithium in tetrahydrofuran 1.) -78 deg C -> 15 deg C, 1.5 h, 2.) -78 deg C -> 20 deg C, overnight;
参考文献
Katritzky, Alan R.; Slawinski, Jaroslaw J.; Brunner, Frederic; Gorun, Sergiu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 1139 - 1145
1: With 1,1'-bis-(diphenylphosphino)ferrocene; N-ethyl-N,N-diisopropylamine in N,N-dimethyl-formamide T=80 - 90°C; 2 h; Inert atmosphere; 2: With hydrogenchloride in water pH=Ca. 4 - 6;
