4,5-二甲基-1H-咪唑合成路线 (共 26 条)
参考文献
Chemische Berichte, , vol. 86, p. 96,107
Chemische Berichte, , vol. 86, p. 88,95
参考文献
Chemische Berichte, , vol. 28, p. 2043
参考文献
Journal of the Chemical Society, , vol. 115, p. 217
反应条件
reagiert analog mit Acetaldehyd und mit Benzaldehyd;
参考文献
Chemische Berichte, , vol. 70, p. 575
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 149, p. 317,319
反应条件
potassium hydroxide in dimethyl sulfoxide T=20 - 65°C; 19 h;
参考文献
Heckenroth, Marion; Neels, Antonia; Garnier, Michael G.; Aebi, Philipp; Ehlers, Andreas W.; Albrecht, Martin
Chemistry - A European Journal, 2009 , vol. 15, # 37 p. 9375 - 9386
反应条件
in benzene T=25°C; KineticsMechanismRate constant;
参考文献
Journal of Organic Chemistry USSR (English Translation), , p. 1470 - 1477
Zhurnal Organicheskoi Khimii, , vol. 16, # 8 p. 1725 - 1732
反应条件
T=550°C; Yield given. Yields of byproduct given;
参考文献
Busby, Reginald E.; Khan, Mohammad A.; Khan, Mohammad R.; Parrick, John; Shaw, C. J. Granville; Iqbal, Mohammad
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1427 - 1430
反应条件
sulfuric acid; nitric acid
参考文献
Fargher; Pyman
Journal of the Chemical Society, 1919 , vol. 115, p. 250
反应条件
1: 52 percent / p-toluenesulfonic acid / Heating 2: 1.) n-BuLi / 1.) THF, hexane, -40 deg C, 30 min; 2.) room temp., overnight 3: H2O / 0.5 h / pH 4 View Scheme
参考文献
Curtis, N.J.; Brown, R.S.
Journal of Organic Chemistry, 1980 , vol. 45, # 20 p. 4038 - 4040
反应条件
sodium methylate in methanol a.) -78 deg C, 1 h, b.) -78 deg C - 23 deg C, 1 h, c.) 23 deg C, 2 h;
参考文献
Kiselyov; Strekowski
Journal of Heterocyclic Chemistry, 1993 , vol. 30, # 5 p. 1361 - 1364