1: 78 percent / hydrazine hydrate / 2 h / Heating
2: 63 percent / sodium nitrite, hydrochloric acid (2M), acetic acid (glacial) / H2O / 1 h / -10 °C
3: 93 percent / toluene / 2.5 h / Heating
4: 8.7 g / sodium hydroxide (20percent) / 60 °C
8: 28.8 g / fluoroboric acid, sodium nitrite / H2O
9: 7.6 g / warming, distillation
10: 1.) lithium / 1.) ether, 2 h
11: decarboxylation
View Scheme
参考文献
Durrani, Aziz A.; Tyman, John H. P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1658 - 1666
