1-溴-4-(苯基磺酰基)苯合成路线 （共 21 条）
反应条件
hexaoxo-.mu.-peroxodisulfate(2-); zirconium oxide T=160°C; Friedel-Crafts reaction; 1 h;
参考文献
Jin, Tongshou; Yang, Mina; Feng, Guoliang; Li, Tongshuang
Journal of Chemical Research - Part S, 2003 , # 11 p. 721 - 723
反应条件
aluminium trichloride
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 30, p. 139
Recueil des Travaux Chimiques des Pays-Bas, , vol. 33, p. 130,152
Chem. Zentralbl., , vol. 85, # I p. 2166
反应条件
in N,N-dimethyl-formamide T=90°C; 24 h; Schlenk techniqueInert atmosphere;
参考文献
Umierski, Natalie; Manolikakes, Georg
Organic Letters, 2013 , vol. 15, # 1 p. 188 - 191
反应条件
in N,N-dimethyl-formamide T=90°C; 24 h; Schlenk techniqueInert atmosphere;
参考文献
Umierski, Natalie; Manolikakes, Georg
Organic Letters, 2013 , vol. 15, # 1 p. 188 - 191
反应条件
sodium hypochlorite; silica gel in dichloromethane; water 0.166667 h; Microwave irradiation; chemoselective reaction;
参考文献
Khurana, Jitender; Nand, Bhaskara
Canadian Journal of Chemistry, 2010 , vol. 88, # 9 p. 906 - 909
反应条件
PEG-400 T=50°C; 0.166667 h; Microwave irradiationSealed tube;
参考文献
Kumar, Dalip; Arun; Pilania, Meenakshi; Shekar, K.P. Chandra
Synlett, 2013 , vol. 24, # 7 art. no. ST-2013-D0144-L, p. 831 - 836
反应条件
bismuth trifluoromethanesulphonate T=120°C; sulfonylation; 5 h; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 64, # 17 p. 6479 - 6482
反应条件
aluminium trichloride
参考文献
Journal of the American Chemical Society, , vol. 74, p. 394,397
反应条件
aluminum oxide; phosphorus pentoxide Friedel-Crafts reaction; 1 h; Heating; Title compound not separated from byproducts;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 180, # 9 p. 2029 - 2034
反应条件
1: 1.) 37percent NaNO2, 20percent aq. H2SO4, 2.) CuBr, 30percent aq. H2SO4 / 1.) 0-4 deg C, 2.) 60 deg C, 1 h 2: 1.) n-BuLi, 2.) water / 1.) Et2O-THF, -60 deg C, 15 min; further reaction times in second step View Scheme
参考文献
Bulletin des Societes Chimiques Belges, , vol. 96, # 1 p. 41 - 50
