2,4-二甲氧基乙酰苯胺合成路线 (共 15 条)
参考文献
Bechhold
Chemische Berichte, 1889 , vol. 22, p. 2377
反应条件
Yield given. Multistep reaction. Title compound not separated from byproducts;
参考文献
Boden, Neville; Bushby, Richard J.; Clark, Leslie D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 543 - 551
反应条件
aluminium trichloride; sodium chloride
T=140°C;
参考文献
Gikas, Evagelos; Parissi-Poulou, Maria; Kazanis, Michael; Vavagianis, Andreas
Synthetic Communications, 2004 , vol. 34, # 22 p. 4233 - 4242
反应条件
1: 100 percent / AlCl3; NaCl / 140 °C
2: 67.6 percent / H2SO4 / H2O / 0 - 5 °C
3: HCl / ethanol / 2 h / Heating
View Scheme
参考文献
Gikas, Evagelos; Parissi-Poulou, Maria; Kazanis, Michael; Vavagianis, Andreas
Synthetic Communications, 2004 , vol. 34, # 22 p. 4233 - 4242
反应条件
[bis(acetoxy)iodo]benzene; silica gel; triethylamine
T=20°C; 5 h;
参考文献
Bodipati, Naganjaneyulu; Peddinti, Rama Krishna
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 23 p. 4549 - 4553