顺-1,3-环己烷二甲酸合成路线 (共 24 条)
反应条件
10 Rh/C; hydrogen in isopropyl alcohol T=60°C; P=760.051 Torr; 24 h; optical yield given as percent de;
参考文献
Chemistry - A European Journal, , vol. 15, # 28 p. 6953 - 6963
反应条件
platinum Hydrogenation;
参考文献
Chemische Berichte, , vol. 51, p. 777
反应条件
nickel T=100°C; P=73550.8 Torr; Hydrogenation.Erwaermen des Reaktionsprodukts mit aethanol. Alkali;
参考文献
Journal of the Chemical Society, , p. 399,402
参考文献
Hulme, Ashley T.; Johnston, Andrea; Florence, Alastair J.; Fernandes, Phillipe; Shankland, Kenneth; Bedford, Colin T.; Welch, Gareth W. A.; Sadiq, Ghazala; Haynes, Delia A.; Motherwell, W. D. Samuel; Tocher, Derek A.; Price, Sarah L.
Journal of the American Chemical Society, 2007 , vol. 129, # 12 p. 3649 - 3657
反应条件
1: acetyl chloride / 1 h / 80 °C 2: 70.92 g / water / Heating View Scheme
参考文献
Journal of the American Chemical Society, , vol. 129, # 12 p. 3649 - 3657
参考文献
Chemische Berichte, , vol. 94, p. 1899 - 1904
反应条件
2: HCl / H2O / 16 h / Heating View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 59, p. 2848 - 2852
反应条件
1: 92 percent / NH2NH2*H2O, KOH / bis-(2-hydroxy-ethyl) ether / 1.) 110 deg C, 1 h; 2.) 180 deg C, 17 h 3: HCl / H2O / 16 h / Heating View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 59, p. 2848 - 2852
反应条件
hydrogenchloride in water 16 h; Heating; Yield given;
参考文献
Canadian Journal of Chemistry, , vol. 59, p. 2848 - 2852
反应条件
1: Cu2Cl2, nPrCO2Na, PdCl2, HC(OMe)3 / 2280 Torr 2: (i) (hydrogenation), (ii) (hydrolysis) View Scheme
参考文献
Journal of Organic Chemistry, , vol. 44, # 2 p. 3474 - 3482