1-(4-乙氧羰基苯基)-2-硫脲合成路线 (共 10 条)
反应条件
sodium hydrogensulfite in water T=80 - 90°C; 1.5 h;
参考文献
Zafar, Abdullah; Melendez, Rosa; Geib, Steven J; Hamilton, Andrew D
Tetrahedron, 2002 , vol. 58, # 4 p. 683 - 690
反应条件
1: acetone / Ambient temperature 2: 2.0 N aq. NaOH / tetrahydrofuran / 3 h / Heating View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 40, # 12 p. 1901 - 1905
反应条件
sodium hydroxide in tetrahydrofuran 3 h; Heating;
参考文献
Journal of Medicinal Chemistry, , vol. 40, # 12 p. 1901 - 1905
反应条件
hydrogenchloride T=80°C; 12 h;
参考文献
Journal of Medicinal Chemistry, , vol. 51, # 5 p. 1242 - 1251
反应条件
1: 85 percent / SOCl2 / 6 h / Heating 2: 38 percent / NaHSO3 / H2O / 1.5 h / 80 - 90 °C View Scheme
参考文献
Tetrahedron, , vol. 58, # 4 p. 683 - 690
参考文献
Journal of the Chemical Society, , p. 440
反应条件
sulfuric acid; chlorobenzene
参考文献
Ukrainskii Khimicheskii Zhurnal (Russian Edition), , vol. 21, p. 344
Chem.Abstr., , p. 14738
反应条件
chloroform; bromine Behandeln des Reaktionsprodukts mit schwefliger Saeure;
参考文献
Dyson; Hunter; Morris
Journal of the Chemical Society, 1927 , p. 1190
反应条件
1: bromine; chloroform / Behandeln des Reaktionsprodukts mit schwefliger Saeure 2: hydrochloric acid View Scheme
参考文献
Dyson; Hunter; Morris
Journal of the Chemical Society, 1927 , p. 1190
反应条件
in ethanol; water 1 h; Heating / reflux;
参考文献
Melvin, JR., Lawrence S.; Graupe, Michael; Venkataramani, Chandrasekar
Patent: US2009/5374 A1, 2009 ;
Location in patent: Page/Page column 156 ;