2-甲基-1-己烯-3-炔合成路线 （共 4 条）
反应条件
triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide in tetrahydrofuran
T=25°C; 3 h;
参考文献
Todo, Hirohisa; Terao, Jun; Watanabe, Hideyuki; Kuniyasu, Hitoshi; Kambe, Nobuaki
Chemical Communications, 2008 , # 11 p. 1332 - 1334
反应条件
1: With bis-triphenylphosphine-palladium(II) chloride; triethylamine
T=20°C; Sonogashira coupling; 0.0833333 h; Inert atmosphere;
2: With copper(l) iodide
Sonogashira coupling; Inert atmosphere;
参考文献
Briones, John F.; Davies, Huw M. L.
Organic Letters, 2011 , vol. 13, # 15 p. 3984 - 3987
参考文献
Priester,W. et al.
Journal of the American Chemical Society, 1976 , vol. 98, p. 8413 - 8421
反应条件
sulfuric acid; mercury(II) oxide
参考文献
Kupin; Petrow
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 3738,3741;engl.Ausg.S.3695,3698
