1,2,3,4四氢- 1 ,4 -亚甲基萘-2,3二醇合成路线 （共 5 条）
反应条件
osmium(VIII) oxide; 4-methylmorpholine N-oxide in water; acetone; butan-1-ol T=25 - 70°C; 2 h; Product distribution / selectivity;
参考文献
Kansal, Vinod Kumar; Ahmad, Suhail; Gupta, Amit
Patent: US2009/318695 A1, 2009 ;
Location in patent: Page/Page column 8 ;
反应条件
in water; acetone; tert-butyl alcohol
参考文献
Wadsworth, Jotham; Palmer, Paige Roanne
Patent: US2002/72524 A1, 2002 ;
反应条件
in water; acetone; tert-butyl alcohol
参考文献
Pfizer Inc
Patent: US6605610 B1, 2003 ;
反应条件
1: 1,2,3,4-tetrahydro-1,4-methano-naphthalene-cis-2,3-diol With sodium periodate; N-benzyl-N,N,N-triethylammonium chloride in dichloromethane; water T=10 - 25°C; 2: benzylamine With sodium tetrahydroborate; acetic acid in dichloromethane T=20 - 25°C; 1 h; 3: With sodium carbonate in dichloromethane; water T=20 - 25°C; pH=8 - 9; 1 h; Product distribution / selectivity;
参考文献
Kansal, Vinod Kumar; Ahmad, Suhail; Gupta, Amit
Patent: US2009/318695 A1, 2009 ;
Location in patent: Page/Page column 8-9 ;
反应条件
in diethyl ether; water
参考文献
Wadsworth, Jotham; Palmer, Paige Roanne
Patent: US2002/72524 A1, 2002 ;
