N-(2,3-二氯苯基)乙酰胺合成路线 （共 18 条）
反应条件
1: HNO3
2: H2SO4
3: SnCl2, aq. HCl
View Scheme
参考文献
Berti,G. et al.
Gazzetta Chimica Italiana, 1977 , vol. 107, p. 175 - 180
反应条件
sulfuric acid; nitric acid
参考文献
Zoecon Corporation
Patent: US4544400 A1, 1985 ;
反应条件
sulfuric acid; potassium nitrate
T=0 - 10°C; Nitration; 4 h; Further byproducts given;
参考文献
Sanna, Paolo; Carta, Antonio; Paglietti, Giuseppe
Heterocycles, 2000 , vol. 53, # 2 p. 423 - 432
参考文献
Holleman
Recueil des Travaux Chimiques des Pays-Bas, 1920 , vol. 39, p. 461
反应条件
1: With sulfuric acid; potassium nitrate
T=2 - 5°C; 4 h;
2: With sulfuric acid
T=100 - 110°C; 2 h;
参考文献
Carta, Antonio; Loriga, Mario; Paglietti, Giuseppe; Ferrone, Marco; Fermeglia, Maurizio; Pricl, Sabrina; Sanna, Tiziana; Ibba, Cristina; La Colla, Paolo; Loddo, Roberta
Bioorganic and Medicinal Chemistry, 2007 , vol. 15, # 5 p. 1914 - 1927
反应条件
sulfuric acid; potassium nitrate
T=0 - 10°C; Nitration; 4 h; Further byproducts given;
参考文献
Sanna, Paolo; Carta, Antonio; Paglietti, Giuseppe
Heterocycles, 2000 , vol. 53, # 2 p. 423 - 432
反应条件
1: 44 percent / KNO3; H2SO4 / 4 h / 0 - 10 °C
2: 87 percent / H2SO4 / 2 h / 100 °C
View Scheme
参考文献
Sanna, Paolo; Carta, Antonio; Paglietti, Giuseppe
Heterocycles, 2000 , vol. 53, # 2 p. 423 - 432
反应条件
tetraphosphorus decasulfide in benzene
Heating;
参考文献
Paramasivam, R.; Ramakrishnan, V. T.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, p. 930 - 934
